天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2009年
5期
776-778,836
,共4页
邓美彩%焦威%董玮玮%鲁润华
鄧美綵%焦威%董瑋瑋%魯潤華
산미채%초위%동위위%로윤화
菊科%橐吾%倍半萜
菊科%橐吾%倍半萜
국과%탁오%배반첩
Compositae%Ligularia fischeri%sesquiterpeniod
从蹄叶橐吾(Ligularia fischeri)的根中分离得到13个化合物,通过波谱学等方法鉴定为2-hydroxplatyphyllide(1),liguhodgsonal(2),ligujapone(3),6'-亚油酰基-β-胡萝卜苷(4),Lupeol(5),6,7-二羟基香豆素(6),β-谷甾醇(7),胡萝卜苷(8),(2S,3S,4R,12E)-N-[2'-(R)-羟基二十二碳酰基]-1,3,4-三羟基-2-氨基-二十碳-12-烯(9),单硬脂酸甘油酯(10),α-羟基二十四烷酸(11),1,3-二棕榈酸甘油酯(12),二十七烷醇(13).其中化合物1~6为首次从该种植物中分离得到.
從蹄葉橐吾(Ligularia fischeri)的根中分離得到13箇化閤物,通過波譜學等方法鑒定為2-hydroxplatyphyllide(1),liguhodgsonal(2),ligujapone(3),6'-亞油酰基-β-鬍蘿蔔苷(4),Lupeol(5),6,7-二羥基香豆素(6),β-穀甾醇(7),鬍蘿蔔苷(8),(2S,3S,4R,12E)-N-[2'-(R)-羥基二十二碳酰基]-1,3,4-三羥基-2-氨基-二十碳-12-烯(9),單硬脂痠甘油酯(10),α-羥基二十四烷痠(11),1,3-二棕櫚痠甘油酯(12),二十七烷醇(13).其中化閤物1~6為首次從該種植物中分離得到.
종제협탁오(Ligularia fischeri)적근중분리득도13개화합물,통과파보학등방법감정위2-hydroxplatyphyllide(1),liguhodgsonal(2),ligujapone(3),6'-아유선기-β-호라복감(4),Lupeol(5),6,7-이간기향두소(6),β-곡치순(7),호라복감(8),(2S,3S,4R,12E)-N-[2'-(R)-간기이십이탄선기]-1,3,4-삼간기-2-안기-이십탄-12-희(9),단경지산감유지(10),α-간기이십사완산(11),1,3-이종려산감유지(12),이십칠완순(13).기중화합물1~6위수차종해충식물중분리득도.
Thirteen known compounds were isolated from the 95% ethanolic extract of roots of Ligularia fischeri. Their structures were elucidatied as 2-hydroxplatyphyllide (1) , liguhodgsonal ( 2), ligujapone ( 3) , 6 '-linoleic-β-daucosterol (4) ,lupeol(5) ,6,7-dihydroxy-coumarin(6), β-sitosterol ( 7), daucosterol (8), (2S,3S,4K, 12E)-N-[2'-( R)-hydroxydocosanoate]-1,3,4-trihydroxy-2-amino-eicosanoate-12-ene ( 9) , monostearin (10), α-hydroxy-lignoceric acid (11) ,1,3-dipalmitin(12) ,hepta-cosanol(13). Among them, 1-6 were isolated from the roots of Ligularia fischeri for the first time.