CAJ | 학술논문

辛基二亚乙基三胺是合成甘氨酸型两性表面活性剂、植物病毒性疾病预防和抑制杀菌剂的重要合成中间体。本文利用正交试验从反应温度、反应时间和反应物料摩尔配比等三个方面，对其进行了合成制备研究，得出了相应的最佳合成工艺条件，结果为：反应温度 160 ℃(一辛基产物)；200 ℃(二辛基产物)；反应时间3 h(一辛基产物)：4 h(二辛基产物)；反应物料摩尔配比4∶1(一辛基产物)；2∶1(二辛基产物)。
신기이아을기삼알시합성감안산형량성표면활성제、식물병독성질병예방화억제살균제적중요합성중간체。본문이용정교시험종반응온도、반응시간화반응물료마이배비등삼개방면，대기진행료합성제비연구，득출료상응적최가합성공예조건，결과위：반응온도 160 ℃(일신기산물)；200 ℃(이신기산물)；반응시간3 h(일신기산물)：4 h(이신기산물)；반응물료마이배비4∶1(일신기산물)；2∶1(이신기산물)。
Octyldiethylenetriamine as an important intermediate was used to synthesize amphoteric surface active agent which belongs to glycines and plant virus diseases'preventing or inhibiting bactericidal agent.According to its reaction temperature,reaction time and mole ratio of reactants, we have carried out an overall study on synthesis of octyldiethylenetriamine through regular-crossed trial,and finally we sum up and get a series of rather good experimental datum.The results as followl: reaction temperature 160 ℃(for mono product); 200 ℃(di-product);reaction times 3 h(for mono-product);4 h(di-product) and mole ratioes of reactants 4∶1(for mono-product) and 2∶1 (di-product).