山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2011年
7期
48-49,63
,共3页
土壤%硼%电感耦合等离子体-原子发射光谱法
土壤%硼%電感耦閤等離子體-原子髮射光譜法
토양%붕%전감우합등리자체-원자발사광보법
soil%boron%inductively coupled plasma atomic emission spectrometric（ ICP - AES）
建立了用ICP—AES测定土壤中硼的分析方法，并对各种最佳分析条件进行探讨。在最佳条件下，用该方法对国家一级标准物质中的痕量硼进行了测定，结果与标准值相符。本法的检出限为0．09mg/kg，精密度为2．30％～4．55％（RSD，n=10），加标回收率为95．0％-103．3％。本方法快速简便，能满足科研及生产中硼的测量要求，尤其适合大批量土壤样品的检测。
建立瞭用ICP—AES測定土壤中硼的分析方法，併對各種最佳分析條件進行探討。在最佳條件下，用該方法對國傢一級標準物質中的痕量硼進行瞭測定，結果與標準值相符。本法的檢齣限為0．09mg/kg，精密度為2．30％～4．55％（RSD，n=10），加標迴收率為95．0％-103．3％。本方法快速簡便，能滿足科研及生產中硼的測量要求，尤其適閤大批量土壤樣品的檢測。
건립료용ICP—AES측정토양중붕적분석방법，병대각충최가분석조건진행탐토。재최가조건하，용해방법대국가일급표준물질중적흔량붕진행료측정，결과여표준치상부。본법적검출한위0．09mg/kg，정밀도위2．30％～4．55％（RSD，n=10），가표회수솔위95．0％-103．3％。본방법쾌속간편，능만족과연급생산중붕적측량요구，우기괄합대비량토양양품적검측。
A method for the determination of boron in soil by inductively coupled plasma atomic emission spectrometric（ ICP -AES） was proposed, and the suitable measurement conditions were optimized by the experiments. Under the optimized conditions, the method had been successfully applied to the determination of boron in a series of national reference materials and the results were in good agreement with the certified values. The detection limit of boron was 0.09mg/kg, and the recovery was 95.0% 103.3% with precision of 2.30%-4.55% （RSD,n = 10）. The results showed that the method was simple, rapid, suitable for determination of boron in soil.
