广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2009年
7期
42-43,68
,共3页
乙烯基三乙氧基硅烷%水解%乙烯基硅树脂%特性粘度
乙烯基三乙氧基硅烷%水解%乙烯基硅樹脂%特性粘度
을희기삼을양기규완%수해%을희기규수지%특성점도
vinyltriethoxylsilane%hydrolysis%vinyl-substituted silicone resin%intrinsic viscosity
以乙烯基三乙氧摹硅烷为原料制备了乙烯基硅树脂,并对影响硅树脂收率和分子量的因素进行了研究.正交实验表明,其适宜的工艺条件是:催化剂(35%～38%浓盐酸)用量为1.5%(体积百分数),反应时间3 h,反应温度在80～85℃.
以乙烯基三乙氧摹硅烷為原料製備瞭乙烯基硅樹脂,併對影響硅樹脂收率和分子量的因素進行瞭研究.正交實驗錶明,其適宜的工藝條件是:催化劑(35%～38%濃鹽痠)用量為1.5%(體積百分數),反應時間3 h,反應溫度在80～85℃.
이을희기삼을양모규완위원료제비료을희기규수지,병대영향규수지수솔화분자량적인소진행료연구.정교실험표명,기괄의적공예조건시:최화제(35%～38%농염산)용량위1.5%(체적백분수),반응시간3 h,반응온도재80～85℃.
Vinyl-substituted silicone resins were prepared by the bydrolyzation of vinyltriethoxylsilane. The influence factors to the yields and intrinsic viscosity of the silicone resin were also studied. The orthogonal experiments showed that the preferable process were: the dosage of hydrochloric acid(35 %-38 %)was 1.5 % (volume ratio), the reaction time was 3 h and the reaction temperature was between 80 ℃ and 85 ℃.
