广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
1期
112-112,104
,共2页
王锐%何嵋%袁晓春%周云%薛梅
王銳%何嵋%袁曉春%週雲%薛梅
왕예%하미%원효춘%주운%설매
复方黄连素片%盐酸小檗碱%TLC-UV法%质量控制
複方黃連素片%鹽痠小檗堿%TLC-UV法%質量控製
복방황련소편%염산소벽감%TLC-UV법%질량공제
compound berberine tablet%berberine hydrochloride%TLC-UV%quality control
采用TLC法将复方黄连素片中的盐酸小檗碱与其它成分分离,定位后,用紫外可见分光光度计测定其含量。TCL-UV法精密度RSD%为1.45%;回收率为98.28%,RSD%为1.73%（n=6）。结果表明,该法高效、灵敏、重现性好,可用作复方黄连素片的质量控制方法。
採用TLC法將複方黃連素片中的鹽痠小檗堿與其它成分分離,定位後,用紫外可見分光光度計測定其含量。TCL-UV法精密度RSD%為1.45%;迴收率為98.28%,RSD%為1.73%（n=6）。結果錶明,該法高效、靈敏、重現性好,可用作複方黃連素片的質量控製方法。
채용TLC법장복방황련소편중적염산소벽감여기타성분분리,정위후,용자외가견분광광도계측정기함량。TCL-UV법정밀도RSD%위1.45%;회수솔위98.28%,RSD%위1.73%（n=6）。결과표명,해법고효、령민、중현성호,가용작복방황련소편적질량공제방법。
Compound berberine tablets were adopted the method of TLC separating berberine hydrochloride and locating it,after which measuring its content with UV spectrophotometer.TLC-UV method accuracy RSD % reached 1.45 %,returns-ratio reached 98.28 %,RSD % 1.73 %（n=6）.The results showed that the TLC-UV method was efficient,sensitive and reproducible.It could be used for the quality of Compound berberine tablets.
