中国医药工业杂志
中國醫藥工業雜誌
중국의약공업잡지
CHINESE JOURNAL OF PHARMACEUTICALS
2010年
2期
88-90
,共3页
程青芳%王启发%许兴友%林俏%刘望军
程青芳%王啟髮%許興友%林俏%劉望軍
정청방%왕계발%허흥우%림초%류망군
3-肉桂酰异阿魏酸苯酯%超声辐射%酯化%合成
3-肉桂酰異阿魏痠苯酯%超聲輻射%酯化%閤成
3-육계선이아위산분지%초성복사%지화%합성
3-cinnamoylisofemlic acid phenyl ester%ultrasonic irradiation%esterification%synthesis
异香(艹卓)醛和肉桂酸经酯化、与丙二酸在微波辐射下经Knoevenagel反应制得3-肉桂酰异阿魏酸后,再在超声波辐射下与取代酚酯化得到3-肉桂酰异阿魏酸苯酯,酯化收率为61%～84%.
異香(艸卓)醛和肉桂痠經酯化、與丙二痠在微波輻射下經Knoevenagel反應製得3-肉桂酰異阿魏痠後,再在超聲波輻射下與取代酚酯化得到3-肉桂酰異阿魏痠苯酯,酯化收率為61%～84%.
이향(초탁)철화육계산경지화、여병이산재미파복사하경Knoevenagel반응제득3-육계선이아위산후,재재초성파복사하여취대분지화득도3-육계선이아위산분지,지화수솔위61%～84%.
3-Cinnamoylisoferulic acid phenyl esters were synthesized from isovanillin and cinnamic acid by esterification and Knoevenagel condensation with malonic acid to afford 3-cinnamoylisoferulic acid,which was subjected to esterification with substituted phenols under ultrasonic irradiation with yields of 61%-84%.
