CAJ | 학술논문

对应用棒状薄层色谱/氢火焰离子化检测器(TLC/FID)测定重油烃族组成(饱和烃、芳烃、胶质)时的影响因素作了探讨。研究发现，在点样及展开过程中，溶剂共挥发可引起样品损失；而且，由于TLC/FID的火焰温度远低于一般GC条件下FID的火焰温度，使不同化合物在FID上的燃烧转化情况有差异，因而其定量校正因子不具有通用性。
대응용봉상박층색보/경화염리자화검측기(TLC/FID)측정중유경족조성(포화경、방경、효질)시적영향인소작료탐토。연구발현，재점양급전개과정중，용제공휘발가인기양품손실；이차，유우TLC/FID적화염온도원저우일반GC조건하FID적화염온도，사불동화합물재FID상적연소전화정황유차이，인이기정량교정인자불구유통용성。
The influencing factors in the determination of hydrocarbons (saturates, aromatics, resins) in heavy oils by thin　layer chromatography/flame ionization detection (TLC/FID) were investigated. It has been found that the solvent co -volatization may cause sample loss during the spotting and developing process, and that the quantitative calibration factors can not be used universally. Because the flame temperature of TLC/FLD is much lower than that of GC/FID, the transformation of different compounds in the flame of FID is varied.