2,5-二[4-(4-溴苯氧基亚甲基)苯基]-1,3,4-噁二唑的合成与表征
2,5-이[4-(4-추분양기아갑기)분기]-1,3,4-오이서적합성여표정
Synthesis and charecterization of 2,5-bis[4-(4-bromophenoxymethylene) phenyl]-I, 3,4-oxadiazole
  • 万方数据
    化工新型材料 화공신형재료
    NEW CHEMICAL MATERIALS
    2009年 12期 40-42 ,共3页

    邓继勇%黄赛金%廖云峰%党丽敏%刘碱

    산계용%황새금%료운봉%당려민%류감

    有机聚合物电致发光材料%噁二唑%单体%合成 有機聚閤物電緻髮光材料%噁二唑%單體%閤成
    유궤취합물전치발광재료%오이서%단체%합성
    organic polymer electrolumineseent material%oxadiazole%monomer%synthesis
    以对甲基苯甲酸、水合肼为原料,通过关环、溴化、醚化合成了一种新型含噁二唑功能基有机聚合物电致发光材料单体2,5-二[4-(4-溴苯氧基亚甲基)苯基]-1,3,4-噁二唑,其化学结构由红外光谱仪及核磁共振氢谱仪进行了表征,产品总收率22.64%.
    이대갑기분갑산、수합정위원료,통과관배、추화、미화합성료일충신형함오이서공능기유궤취합물전치발광재료단체2,5-이[4-(4-추분양기아갑기)분기]-1,3,4-오이서,기화학결구유홍외광보의급핵자공진경보의진행료표정,산품총수솔22.64%.
    Using methylparaben and hydrazine hydrate as raw materials, by closing ring, bromination, etherifica-tion, a novel oxadiazole-functionalized monomer of organic polymer electroluminescent materials 2,5-bis[4-(4-bromophe-noxymethylene)-1, 3,4-oxadiazole was synthesized, it's molecular structure was characterized by IR and ~1H NMR.The o-verall yield of the product was 22. 64%.
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