中医药学报
中醫藥學報
중의약학보
ACTA CHINESE MEDICINE AND PHARMACOLOGY
2009年
3期
52-54
,共3页
钮旭升%陶树青%马志强%宋少江
鈕旭升%陶樹青%馬誌彊%宋少江
뉴욱승%도수청%마지강%송소강
药物化学%结构鉴定%核磁共振波谱%辽东楤木%三萜皂苷
藥物化學%結構鑒定%覈磁共振波譜%遼東楤木%三萜皂苷
약물화학%결구감정%핵자공진파보%료동송목%삼첩조감
目的:研究辽东槐木Amlia elata.(Miq.)Seem芽提取物(总皂苷)中的化学成分.方法:利用硅胶柱色谱、制备高效液相柱色谱进行分离纯化,根据理化性质和光谱数据进行结构鉴定.结果:得到5个五环三萜皂苷,分别鉴定为araloside A(1),araloside C(2),楤皂苷X V(3,congmunoside X V),3-O-[(-D-glueopyranosyl(1→3)-(-D-glucopyranosyl]oleanolic acid 28-O-(-D-glucopyranoside(4)和3-O-[(-D-glucopyranosyl(1→2)-(-D-glucopyranosyl]hederagenin(5).结论:化合物4和5为首次从该属植物中分得.
目的:研究遼東槐木Amlia elata.(Miq.)Seem芽提取物(總皂苷)中的化學成分.方法:利用硅膠柱色譜、製備高效液相柱色譜進行分離純化,根據理化性質和光譜數據進行結構鑒定.結果:得到5箇五環三萜皂苷,分彆鑒定為araloside A(1),araloside C(2),楤皂苷X V(3,congmunoside X V),3-O-[(-D-glueopyranosyl(1→3)-(-D-glucopyranosyl]oleanolic acid 28-O-(-D-glucopyranoside(4)和3-O-[(-D-glucopyranosyl(1→2)-(-D-glucopyranosyl]hederagenin(5).結論:化閤物4和5為首次從該屬植物中分得.
목적:연구료동괴목Amlia elata.(Miq.)Seem아제취물(총조감)중적화학성분.방법:이용규효주색보、제비고효액상주색보진행분리순화,근거이화성질화광보수거진행결구감정.결과:득도5개오배삼첩조감,분별감정위araloside A(1),araloside C(2),송조감X V(3,congmunoside X V),3-O-[(-D-glueopyranosyl(1→3)-(-D-glucopyranosyl]oleanolic acid 28-O-(-D-glucopyranoside(4)화3-O-[(-D-glucopyranosyl(1→2)-(-D-glucopyranosyl]hederagenin(5).결론:화합물4화5위수차종해속식물중분득.
