苏州大学学报（自然科学版）
囌州大學學報（自然科學版）
소주대학학보（자연과학판）
JOURNAL OF SUZHOU UNIVERSITY(NATURAL SCIENCE)
2005年
3期
59-62
,共4页
三氮唑%晶体结构%合成
三氮唑%晶體結構%閤成
삼담서%정체결구%합성
Triazole%crystal structure%synthesis
合成了化合物1,4-二(1,2,4-三氮唑-1-)丁烷并且测定了其晶体结构. 晶体数据:C8H12N6, 单斜晶系, 空间群P21／c,a=0.788 47(19)nm,b=0.901 4(2)nm, c = 0.706 68(19)nm,β = 105.994(6)°V = 0.482 8(2)nm3,Mr =192.24, Z = 2, Dc = 1.322 g/cm3, F(000) = 204, μ(Mo K(a))= 0.090 mm-1,R = 0.058 8, wR = 0.173 8.
閤成瞭化閤物1,4-二(1,2,4-三氮唑-1-)丁烷併且測定瞭其晶體結構. 晶體數據:C8H12N6, 單斜晶繫, 空間群P21／c,a=0.788 47(19)nm,b=0.901 4(2)nm, c = 0.706 68(19)nm,β = 105.994(6)°V = 0.482 8(2)nm3,Mr =192.24, Z = 2, Dc = 1.322 g/cm3, F(000) = 204, μ(Mo K(a))= 0.090 mm-1,R = 0.058 8, wR = 0.173 8.
합성료화합물1,4-이(1,2,4-삼담서-1-)정완병차측정료기정체결구. 정체수거:C8H12N6, 단사정계, 공간군P21／c,a=0.788 47(19)nm,b=0.901 4(2)nm, c = 0.706 68(19)nm,β = 105.994(6)°V = 0.482 8(2)nm3,Mr =192.24, Z = 2, Dc = 1.322 g/cm3, F(000) = 204, μ(Mo K(a))= 0.090 mm-1,R = 0.058 8, wR = 0.173 8.
The title compound 1,4-bis(1,2,4-triazol-1-yl)butane has been synthesized and its structure was determined by single-crystal X-ray diffraction. Crystal data: C8H12N6, mono-clinic, space group P21／c, a =0.788 47(19)nm, b =0.901 4(2)nm,c =0.706 68(19)nm,β= 105.994(6)°V =0.482.8(2)nm3,Mr = 192.24, Z = 2, Dc = 1.322 g／cm3, F(000) = 204,μ(Mo K(a)) = 0.090 mm-1, the final R =0.058 8 and wR = 0.173 8 for 800 observed reflections (I＞ 2σ(I)).
