中国现代应用药学
中國現代應用藥學
중국현대응용약학
CONTENTS IN BRIEF
2001年
1期
61-62
,共2页
陈桂云%陈琴鸣%王泽英%丁以华
陳桂雲%陳琴鳴%王澤英%丁以華
진계운%진금명%왕택영%정이화
齐墩果酸%三两半药酒%高效液相色谱法
齊墩果痠%三兩半藥酒%高效液相色譜法
제돈과산%삼량반약주%고효액상색보법
目的:建立三两半药酒中齐墩果酸含量测定方法。方法:HPLC法,以Hypersil(4.6×250mm,5μm)为色谱柱,甲醇-水(90∶10)为流动相,检测波长为220nm。结果:齐墩果酸测定线性范围为9.6~48.0μg/ml(r=0.9998),平均回收率为98.5%。结论:该法简便,可用于测定三两半药酒中齐墩果酸的含量。
目的:建立三兩半藥酒中齊墩果痠含量測定方法。方法:HPLC法,以Hypersil(4.6×250mm,5μm)為色譜柱,甲醇-水(90∶10)為流動相,檢測波長為220nm。結果:齊墩果痠測定線性範圍為9.6~48.0μg/ml(r=0.9998),平均迴收率為98.5%。結論:該法簡便,可用于測定三兩半藥酒中齊墩果痠的含量。
목적:건립삼량반약주중제돈과산함량측정방법。방법:HPLC법,이Hypersil(4.6×250mm,5μm)위색보주,갑순-수(90∶10)위류동상,검측파장위220nm。결과:제돈과산측정선성범위위9.6~48.0μg/ml(r=0.9998),평균회수솔위98.5%。결론:해법간편,가용우측정삼량반약주중제돈과산적함량。
OBJECTIVE:To develope a method for the determination of olesnolic acid in Sanliangban Yaojiu.METHOD:HPLC was employed.The column was Hyperisil ODS(4.6×250mm,5μm),the mobile phase was methanol-water(90∶10),and the detection wavelength was 220nm.RESULTS:The linear range was from 9.6 to 48.0μg/ml(r=0.9998),and the average recovery was 98.5%.CONCLUSION:The method is simple for the determination of oleanolic acid in Sanliangban Yaojiu.