CAJ | 학술논문

运用各种色谱分离方法对藏东瑞香(Daphne bholua)地上部分的乙醇提取物进行分离纯化,从中分离得到12个化合物.通过波谱学数据并与已知化合物数据作比较,它们分别鉴定为:木犀草素(1)、芫花素(2)、芫花素5-O-β-D-葡萄糖苷(3)、3'-羟基-芫花素(4)、3'-甲氧基-芫花素(5)、异新狼毒素(6)、Genkwanol B(7)、Oleodaphnone(8)、阿魏醛(9)、香草醛(10)、对羟基苯甲酸乙酯(11)、β-谷甾醇(12).所有这些化合物都为从该植物中首次分离鉴定.
운용각충색보분리방법대장동서향(Daphne bholua)지상부분적을순제취물진행분리순화,종중분리득도12개화합물.통과파보학수거병여이지화합물수거작비교,타문분별감정위:목서초소(1)、원화소(2)、원화소5-O-β-D-포도당감(3)、3'-간기-원화소(4)、3'-갑양기-원화소(5)、이신랑독소(6)、Genkwanol B(7)、Oleodaphnone(8)、아위철(9)、향초철(10)、대간기분갑산을지(11)、β-곡치순(12).소유저사화합물도위종해식물중수차분리감정.
Different column chromatography methods were used in a search for compounds in the plant Daphne bholua. Ethanol extract of the aerial parts of the plant has resulted in the isolation of twelve compounds. Based on ESI-MS and NMR spectra data,they were identified as luteolin(1) ,genkwanin(2) ,genkwanin 5-O-β-D-glucopyranoside(3) ,3'-hy-droxy-genkwanin(4) ,velutin(5) ,isoneochamaejasmin A(6) ,genkwanol B(7) ,oleodaphnone(8) ,ferulaldehyde(9), vanillin (10) ,ethylparaben( 11) ,β-sitosterol( 12). All these compounds were isolated from this plant for the first time.