陕西师范大学学报(自然科学版)
陝西師範大學學報(自然科學版)
협서사범대학학보(자연과학판)
JOURNAL OF SHAANXI NORMAL UNIVERSITY(NATURAL SCIENCE EDITION)
2010年
1期
70-74
,共5页
魏希颖%徐慧娴%杨小军%陈康健%张玲%葛茜%曾成鸣
魏希穎%徐慧嫻%楊小軍%陳康健%張玲%葛茜%曾成鳴
위희영%서혜한%양소군%진강건%장령%갈천%증성명
连翘种子油%GC-MS分析%抗氧化活性
連翹種子油%GC-MS分析%抗氧化活性
련교충자유%GC-MS분석%항양화활성
essential oil from seeds of Forsythia suspense (Thunb.) Vahl.%GC-MS%antioxidantive activitie
利用GC-MS联用技术对连翘种子油成分进行分析,各成分的质谱图与标准谱对照,分离鉴定出63种化合物,其中萜类化舍物占70%以上.所鉴定成分的含量占全油的98.91%.主要成分为β-蒎烯(47.78%),其次是β-水芹烯(14.91%)和α-蒎烯(14.02%),另检测出0.76%的含碘化合物和0.55%的含硅化合物等.用DPPH法和邻苯三酚自氧化法测定其抗氧化活性,结果发现其对有机自由基(DPPH)和超氧阴离子自由基(O_2~-)均有显著清除作用,清除率高达90%以上.
利用GC-MS聯用技術對連翹種子油成分進行分析,各成分的質譜圖與標準譜對照,分離鑒定齣63種化閤物,其中萜類化捨物佔70%以上.所鑒定成分的含量佔全油的98.91%.主要成分為β-蒎烯(47.78%),其次是β-水芹烯(14.91%)和α-蒎烯(14.02%),另檢測齣0.76%的含碘化閤物和0.55%的含硅化閤物等.用DPPH法和鄰苯三酚自氧化法測定其抗氧化活性,結果髮現其對有機自由基(DPPH)和超氧陰離子自由基(O_2~-)均有顯著清除作用,清除率高達90%以上.
이용GC-MS련용기술대련교충자유성분진행분석,각성분적질보도여표준보대조,분리감정출63충화합물,기중첩류화사물점70%이상.소감정성분적함량점전유적98.91%.주요성분위β-파희(47.78%),기차시β-수근희(14.91%)화α-파희(14.02%),령검측출0.76%적함전화합물화0.55%적함규화합물등.용DPPH법화린분삼분자양화법측정기항양화활성,결과발현기대유궤자유기(DPPH)화초양음리자자유기(O_2~-)균유현저청제작용,청제솔고체90%이상.
The essential oil from seeds of Forsythia suspense (Thunb.) Vahl. was analyzed by GC-MS, and 63 components were identified by comparision with the standard mass spectrogram. Among of the components, the terpenoid was more then 70 percent. The content of indentified componenes was 98.91 percent of the whole oil. The main chemical components of the oil were β-Pinene(47. 78%), β-Phellandrene (14. 91%) and a-Pinene (14. 02%). The iodine and silicon components were also identified in 0.76% and 0.55%, respectively. The antioxidant activities of the oil were assayed through scavenging effects to DPPH and superoxide anion free radical (O_2~-). The results indicated that essential oil from seeds of Forsythia suspense (Thunb.) Vahl. showed much high antioxidant activity and the scavenging effects to DPPH and (O_2~-) were more than 90%. The study could provide theoretical foundation for further studying and developing of the essential oil from seeds of Forsythia suspense (Thunb.) Vahl.