CAJ | 학술논문

通过利用Pt(IV)-GICs和Pt(IV)乙炔黑层间化合物来制备应用于甲醇电氧化石墨和乙炔黑载铂催化剂。具体过程如下：在惰性气氛下，利用H2PtCl6与石墨和乙炔黑反应制备层间化合物，再将层间化合物分别进行热解和化学还原。结果表明，利用热解法制备的载体催化剂对甲醇电化学氧化具有很好的活性。
통과이용Pt(IV)-GICs화Pt(IV)을결흑층간화합물래제비응용우갑순전양화석묵화을결흑재박최화제。구체과정여하：재타성기분하，이용H2PtCl6여석묵화을결흑반응제비층간화합물，재장층간화합물분별진행열해화화학환원。결과표명，이용열해법제비적재체최화제대갑순전화학양화구유흔호적활성。
Anode catalysts for methanol oxidation were prepared bysubsequent reduction of Pt(IV) chloride-graphite intercalation compounds (GICs) and Pt(IV) chloride-acetylene black intercalation compounds. The intercalation compounds were obtained by the reaction of H2PtCl6 with graphite and acetylene black respectively under an inert atmosphere. Two methods were employed in preparation of carbon supported platinum catalysts from intercalation compounds: one was pyrolysis and another chemical method. The activity of catalytics from pyrolysis is higher than that from chemical reduction.