天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2003年
5期
383-386
,共4页
童孝田%谭昌恒%马晓强%蒋山好%朱大元
童孝田%譚昌恆%馬曉彊%蔣山好%硃大元
동효전%담창항%마효강%장산호%주대원
石松生物碱%东北石杉%分离
石鬆生物堿%東北石杉%分離
석송생물감%동북석삼%분리
Lycopodium alkaloids%Huperzia miyoshiana%isolation
从东北石杉中分离得到7个石松生物碱,通过NMR、MS及IR等光谱分析,分别鉴定为:luciduline( 1 ), dithydroluciduline(2 ), lycodine (3), huperzine B ( 4 ), serratinine ( 5 ), serratidine ( 6 ), mecleanine(7).这些化合物均为首次从该植物中分得.
從東北石杉中分離得到7箇石鬆生物堿,通過NMR、MS及IR等光譜分析,分彆鑒定為:luciduline( 1 ), dithydroluciduline(2 ), lycodine (3), huperzine B ( 4 ), serratinine ( 5 ), serratidine ( 6 ), mecleanine(7).這些化閤物均為首次從該植物中分得.
종동북석삼중분리득도7개석송생물감,통과NMR、MS급IR등광보분석,분별감정위:luciduline( 1 ), dithydroluciduline(2 ), lycodine (3), huperzine B ( 4 ), serratinine ( 5 ), serratidine ( 6 ), mecleanine(7).저사화합물균위수차종해식물중분득.
Seven known Lycopodium alkaloids were isolated for the first time from Huperzia Miyoshiana (Makino) Ching (Huperziaceae). Their structures were identified as luciduline (1), dihydroluciduline (2), lycodine (3), huperzine B (4), serratinine (5), serratidine (6), macleanine (7), respectively, on the basis of spectral evidences.