结构化学
結構化學
결구화학
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
2003年
6期
643-646
,共4页
罗悔%马怀柱%苏庆德%刘青山
囉悔%馬懷柱%囌慶德%劉青山
라회%마부주%소경덕%류청산
bis-9-fluorenylmethylphenyl silane%synthesis%crystal structure
The title compound bis-9-fluorenylmethylphenyl silane (C33H26Si, Mr = 450.63) was synthesized and its structure has been synthesized and determined by X-ray analysis. The crystal is of triclinic, space group Pī with a = 9.478(1), b = 10.0956(1), c = 13.0243(2)(A°),α= 92.668(2),β= 90.809(2),γ= 99.348(2)°,λ= 0.71073(A°),μ(MoKα)= 0.115 mm-1, V = 1288.1(2)(A°)3, Z = 2, Dc = 1.219 g/cm3 and F(000) = 476. The structure was refined to R = 0.0437 and wR(F2) = 0.0963 for 3346 observed reflections with I>2σ(I). X-ray diffraction analysis reveals that the title compound is bis-9-fluorenylmethylphenyl silane.
