兴义民族师范学院学报
興義民族師範學院學報
흥의민족사범학원학보
JOURNAL OF SOUTHWEST GUIZHOU TEACHERS'COLLEGE OF NATIONALITIES
2011年
3期
118-120
,共3页
9-(2-苯并咪唑基)壬酸盐酸盐%晶体结构
9-(2-苯併咪唑基)壬痠鹽痠鹽%晶體結構
9-(2-분병미서기)임산염산염%정체결구
9-(1H-benzo[d]imidazol-2-yl)nonanoic acid chloride hydrate%Crystal structure
以邻苯二胺和1,10-癸二酸为原料,在4 mol/L盐酸中反应制备新化合物9-(2-苯并咪唑基)壬酸盐酸盐水合物,利用X-射线衍射法测定其晶体结构。晶体数据:单斜晶系,空间群P21/c,a=0.80033(12)nm,b=4.2375(6)nm,c=0.52327(8)nm,α=90°,β=91.170(5)°,γ=90°,V=1.7742(5)nm3,Z=4。
以鄰苯二胺和1,10-癸二痠為原料,在4 mol/L鹽痠中反應製備新化閤物9-(2-苯併咪唑基)壬痠鹽痠鹽水閤物,利用X-射線衍射法測定其晶體結構。晶體數據:單斜晶繫,空間群P21/c,a=0.80033(12)nm,b=4.2375(6)nm,c=0.52327(8)nm,α=90°,β=91.170(5)°,γ=90°,V=1.7742(5)nm3,Z=4。
이린분이알화1,10-계이산위원료,재4 mol/L염산중반응제비신화합물9-(2-분병미서기)임산염산염수합물,이용X-사선연사법측정기정체결구。정체수거:단사정계,공간군P21/c,a=0.80033(12)nm,b=4.2375(6)nm,c=0.52327(8)nm,α=90°,β=91.170(5)°,γ=90°,V=1.7742(5)nm3,Z=4。
9-(1H-benzo[d]imidazol-2-yl)nonanoic acid chloride hydrate as a novel compound was prepared in a solution of 4M HCl through the material of o-phenylenedimine and 1,10-decanedicarboxylic acid.The title compound was characterized by single X-ray diffraction,crystal data for title compound: L:monochnic,space group P21/c,a=0.80033(12) nm,b=4.2375(6) nm,c=0.52327(8) nm,α=90°,β=91.170(5) °,γ=90°V=1.7742(5) nm3,Z=4.