CAJ | 학술논문

目的研究冬青科植物毛冬青Ilex pubescens Hook. et Arn.根的化学成分.方法运用多种层析分离方法进行分离纯化,通过理化常数和波谱数据确定化合物的结构.结果从毛冬青根中分离并鉴定了12个化合物,分别为ilexoside D(1);ilexgenin A(2);spinasterol(3);(+)-fraxiresinol-1-O-β-D-glucoside(4);liriodendrin(5);tortoside A(6);magnolenin C(7);丁香苷(8);sinapic aldehyde 4-O-β-D-glucopyranoside(9);4,5-di-O-caffeoylquinic acid(10);β-谷甾醇(11)和β-胡萝卜苷(12).结论化合物3,4,10为首次从该属植物中分离得到.
목적 연구동청과식물모동청Ilex pubescens Hook. et Arn.근적화학성분.방법 운용다충층석분리방법진행분리순화,통과이화상수화파보수거학정화합물적결구.결과 종모동청근중분리병감정료12개화합물,분별위ilexoside D(1);ilexgenin A(2);spinasterol(3);(+)-fraxiresinol-1-O-β-D-glucoside(4);liriodendrin(5);tortoside A(6);magnolenin C(7);정향감(8);sinapic aldehyde 4-O-β-D-glucopyranoside(9);4,5-di-O-caffeoylquinic acid(10);β-곡치순(11)화β-호라복감(12).결론 화합물3,4,10위수차종해속식물중분리득도.
Objective To study the chemical constituents of the roots of Ilex pubescens Hook. et Arn. Methods Chemical constituents were isolated and purified by several column chromatographic methods. The structures were identified by physicochemical properties and spectral data.Results Twelve compounds were isolated from the plant. Their structures were identified as ilexoside D(1), ilexgenin A(2), spinasterol(3), (+)-fraxiresinol-1-O-β-D-glucoside (4), liriodendrin (5), tortoside A(6), magnolenin C(7), syningin(8), sinapic aldehyde 4-O-β-D-glucopyrano- side(9), 4,5-di-O-caffeoylquinic acid(10), β-sitosterol(11) and β-daucosterol(12), respectively. Conclusion Compounds 3, 4 and 10 were isolated from this plant for the first time.