材料导报
材料導報
재료도보
MATERIALS REVIEW
2009年
z1期
63-65,78
,共4页
张绍岩%次立杰%张星辰%陈丁龙
張紹巖%次立傑%張星辰%陳丁龍
장소암%차립걸%장성신%진정룡
纳米Al2O3%纳米SiO2%釉料%烧结
納米Al2O3%納米SiO2%釉料%燒結
납미Al2O3%납미SiO2%유료%소결
nano-Al2O3%nano-SiO2%glaze%sintering
以普通无机盐为原料采用沉淀法制备了纳米Al2O3和SiO2.XRD分析表明样品为无定形结构,SEM分析表明得到的纳米Al2O3和SiO2均为球形颗粒,直径分别为90m和300nm.将合成的纳米材料添加至陶瓷面釉进行烧结测试,结果表明,添加纳米材料釉料的烧结温度比普通釉料的烧结温度降低了30℃,釉层性能明显得到改善,釉料良好的性能源于纳米材料较大的表面积及高的烧结活性.
以普通無機鹽為原料採用沉澱法製備瞭納米Al2O3和SiO2.XRD分析錶明樣品為無定形結構,SEM分析錶明得到的納米Al2O3和SiO2均為毬形顆粒,直徑分彆為90m和300nm.將閤成的納米材料添加至陶瓷麵釉進行燒結測試,結果錶明,添加納米材料釉料的燒結溫度比普通釉料的燒結溫度降低瞭30℃,釉層性能明顯得到改善,釉料良好的性能源于納米材料較大的錶麵積及高的燒結活性.
이보통무궤염위원료채용침정법제비료납미Al2O3화SiO2.XRD분석표명양품위무정형결구,SEM분석표명득도적납미Al2O3화SiO2균위구형과립,직경분별위90m화300nm.장합성적납미재료첨가지도자면유진행소결측시,결과표명,첨가납미재료유료적소결온도비보통유료적소결온도강저료30℃,유층성능명현득도개선,유료량호적성능원우납미재료교대적표면적급고적소결활성.
Using inorganic salts as raw materials,Al2O3 and SiO2 nanoparticles are fabricated by simple and facile chemical precipitation.The structure and morphologies of the as-synthesized Al2O3 and SiO2 products are characterized by Xray diffraction(XRD) and scanning electron microscopy(SEM).The results show that the products are amorphous and the diameters of the Al2O3 and SiO2 particles are about 90 nm and 300 nm respectively.Furthermore,the as-prepared Al2O3 and SiO2 nanoparticles are applied and examined for the additives in the traditional glaze.The results show that the sintering characteristic of glaze is improved and the sintering temperature can be decreased by 30℃ by using Al2O3 and SiO2 nanoparticles as the additives.The improved performance may arise from relatively high specific surface areas and sintering activity of the nanostructured materials.