化学研究与应用
化學研究與應用
화학연구여응용
CHEMICAL RESEARCH AND APPLICATION
2010年
4期
511-513
,共3页
芳酰基芳基偶氮化合物%芳酰基芳肼类化合物%水合肼%还原
芳酰基芳基偶氮化閤物%芳酰基芳肼類化閤物%水閤肼%還原
방선기방기우담화합물%방선기방정류화합물%수합정%환원
acyl-diazene compounds%diaryl acylhydrazine compounds%NH_2NH_2·H_2O%reduction
Six diaryl acylhydrazine compounds were synthesized in normal temperature with self-made acyl-diazene compounds as raw materials and NH_2NH_2·H_2O as reducer.The products were confirmed by means of elemental analysis,IR and~1H NMR.In the results of IR,there were two N-H absorption at approximately 3200 and 3400 cm~(-1).However,the absorptions of N=N in raw materials disappeared.In the results of 1H NMR,the N-H chemical shifts couldn't be found.Meanwhile,two N-H chemical shifts were detected about from 8.46 to 11.38,respectively.The results of products' elemental analysis were consistent with the theoretical values.The yields of those six products were about from 84% to 93%.
