6-溴-1，3-苯并二恶茂-4-甲醛的合成
6-추-1，3-분병이악무-4-갑철적합성
SYNTHESIS OF 6-BROMO- 1 , 3-BENZODIOXOLE- 4-CARBONALDEHYDE
  • 万方数据
    四川大学学报(自然科学版) 사천대학학보(자연과학판)
    JOURNAL OF SICHUAN UNIVERSITY
    2000年 3期 474-476 ,共3页

    敖波%彭强%赵为%杨占坤%蔡雅棠%朱家理%谢明贵

    오파%팽강%조위%양점곤%채아당%주가리%사명귀



    6-bromo- 1,3-benzodiozole-4-carbonaldehyde,synthesis,methylenation


    The 6-bromo- 1, 3- benzodiozole- 4- carbonaldehyde was synthesized by using 2- hydroxy-3-methoxy benzaldehyde as an original reactant, through three steps of bromination, demethylation and methylenation. The title compound was identified by elemental analysis. IR, 1HNMR and MS. The melting point was 113-114℃ determined with macroscope melting instrument and was 113.8C determined with DSC.
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