波谱学杂志
波譜學雜誌
파보학잡지
CHINESE JOURNAL OF MAGNETIC RESONANCE
2005年
1期
1-5
,共5页
张起辉%高慧媛%周莲娣%韩志超%吴立军
張起輝%高慧媛%週蓮娣%韓誌超%吳立軍
장기휘%고혜원%주련제%한지초%오립군
核磁共振%二维核磁共振%吴茱萸%吴茱萸内酯%结构
覈磁共振%二維覈磁共振%吳茱萸%吳茱萸內酯%結構
핵자공진%이유핵자공진%오수유%오수유내지%결구
NMR%2D NMR%Evodia rutaecarpa%Limonin%Structure
从吴茱萸Evodia Rutaecarpa (Juss.) Benth.中分离得到并鉴定了化合物吴茱萸内酯,我们应用二维核磁技术首次对化合物吴茱萸内酯的核磁信号进行了准确归属,并纠正了文献中部分氢信号归属的错误.
從吳茱萸Evodia Rutaecarpa (Juss.) Benth.中分離得到併鑒定瞭化閤物吳茱萸內酯,我們應用二維覈磁技術首次對化閤物吳茱萸內酯的覈磁信號進行瞭準確歸屬,併糾正瞭文獻中部分氫信號歸屬的錯誤.
종오수유Evodia Rutaecarpa (Juss.) Benth.중분리득도병감정료화합물오수유내지,아문응용이유핵자기술수차대화합물오수유내지적핵자신호진행료준학귀속,병규정료문헌중부분경신호귀속적착오.
A compound was isolated from Evodia rutaecarpa and identified to be Limonin. The NMR signals of the compound were assigned by 2D NMR. The results show that the assignment of some proton signals made in the previous studies was erroneous. Correction was made for the incorrect assignment.
