波谱学杂志
波譜學雜誌
파보학잡지
CHINESE JOURNAL OF MAGNETIC RESONANCE
2011年
3期
390-398
,共9页
朱传钧%朱美玲%崔育新%姜标%郑锦鸿
硃傳鈞%硃美玲%崔育新%薑標%鄭錦鴻
주전균%주미령%최육신%강표%정금홍
核磁共振%指认%二维核磁共振%(E)-3-(4-羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物%构象分析
覈磁共振%指認%二維覈磁共振%(E)-3-(4-羥苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物%構象分析
핵자공진%지인%이유핵자공진%(E)-3-(4-간분기)-1-(고정-1-기)병-2-희-1-동연생물%구상분석
NMR%assignment%2D NMR%(E)-3-(4-hydroxyphenyl)-l-(piperidin-l-yl) prop-2-en-l-one derivatives%conformational analysis
设计并合成了-系列(E)-3-(4-羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物.通过一维和二维核磁共振实验完成了1 H和13C信号的指认.通过ROESY、变温实验和分子模拟技术对这类化合物的构象进行了分析.
設計併閤成瞭-繫列(E)-3-(4-羥苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物.通過一維和二維覈磁共振實驗完成瞭1 H和13C信號的指認.通過ROESY、變溫實驗和分子模擬技術對這類化閤物的構象進行瞭分析.
설계병합성료-계렬(E)-3-(4-간분기)-1-(고정-1-기)병-2-희-1-동연생물.통과일유화이유핵자공진실험완성료1 H화13C신호적지인.통과ROESY、변온실험화분자모의기술대저류화합물적구상진행료분석.
A new series of ( E)-3- ( 4-hydroxyphenyl)-l- (piperidin-l-yl) prop-2-en- 1-one derivatives were designed and synthesized.1 H and 13C NMR spectral assignments of these compounds were presented by one- and two- dimensional NMR experiments and conformations were analyzed by ROESY,variable-temperature NMR spectroscopy and molecular modeling.
