齐鲁石油化工
齊魯石油化工
제로석유화공
QILU PETROCHEMICAL TECHNOLOGY
2011年
3期
215-218
,共4页
吸附甲乙酮尾气%氢气%净化
吸附甲乙酮尾氣%氫氣%淨化
흡부갑을동미기%경기%정화
adsorption%MEK tail - gas%hydrogen%purltication
针对泰州石化公司甲乙酮装置尾气的组成特点,采用前冷却、吸附流程回收其中的氢气。通过冷却脱除尾气中夹带的液体和部分高碳醇;采用三塔吸附操作,在常温下脱除尾气中甲乙酮、仲丁醇及C4组分,高温下使吸附剂再生。装置标定结果表明,氢气的体积分数达到99.99%,回收率高达93.75%。
針對泰州石化公司甲乙酮裝置尾氣的組成特點,採用前冷卻、吸附流程迴收其中的氫氣。通過冷卻脫除尾氣中夾帶的液體和部分高碳醇;採用三塔吸附操作,在常溫下脫除尾氣中甲乙酮、仲丁醇及C4組分,高溫下使吸附劑再生。裝置標定結果錶明,氫氣的體積分數達到99.99%,迴收率高達93.75%。
침대태주석화공사갑을동장치미기적조성특점,채용전냉각、흡부류정회수기중적경기。통과냉각탈제미기중협대적액체화부분고탄순;채용삼탑흡부조작,재상온하탈제미기중갑을동、중정순급C4조분,고온하사흡부제재생。장치표정결과표명,경기적체적분수체도99.99%,회수솔고체93.75%。
According to the composition of tail gas in methyl ethyl ketone device, hydrogen was recovered by cooling process before absorption recovery. Liquid and part of higher alcohols v/ere removed from tail - gas in cooling system, methyl ethyl ketone, see - butyl alcohol and C4 components were removed with three absorption towers at room temperature, while adsorbent was regenerated at high temperature. The volume fraction and recovery rate of product hydrogen reached 99. 99% and 93.75%, respectively.