金属学报
金屬學報
금속학보
ACTA METALLURGICA SINICA
2009年
11期
1364-1369
,共6页
贾玉贤%金涛%刘金来%孙晓峰%胡壮麒
賈玉賢%金濤%劉金來%孫曉峰%鬍壯麒
가옥현%금도%류금래%손효봉%호장기
镍基单品高温合金%蠕变%各向异性%晶体取向
鎳基單品高溫閤金%蠕變%各嚮異性%晶體取嚮
얼기단품고온합금%연변%각향이성%정체취향
Ni based single crystal superalloy%creep%anisotropy%crystal orientation
分别制备了[001]和[011]取向的Ni-Co-Cr-Mo-w-Al-Ti-Ta镍基单晶高温合金试样.在750℃/750 MPa条件下,[001]取向合金的平均蠕变寿命叫显高于[011]取向合金,[011]取向合金延伸率稍高.在982℃/248 MPa条件下,[001]取向合金的平均蠕变寿命和延伸率均高于[011]取向合金,各向异性上要表现在加速蠕变阶段,但各向异性程度比低温高应力时显著降低.存高温低应力条件下,2种取向合金中γ'相均已形筏,[001]取向合金的筏化方向垂直于应力轴,而[011]取向合金的筏化方向与应力轴的夹角约为45°.γ'相形筏后,阻碍了位错运动,导致加工硬化,因此,γ'相筏化是各向异性程度降低的主要原因.在[011]取向合金的蠕变后期观察到挛品组织同时穿越γ和γ'相,导致试样塑性人幅度降低,迅速断裂.
分彆製備瞭[001]和[011]取嚮的Ni-Co-Cr-Mo-w-Al-Ti-Ta鎳基單晶高溫閤金試樣.在750℃/750 MPa條件下,[001]取嚮閤金的平均蠕變壽命叫顯高于[011]取嚮閤金,[011]取嚮閤金延伸率稍高.在982℃/248 MPa條件下,[001]取嚮閤金的平均蠕變壽命和延伸率均高于[011]取嚮閤金,各嚮異性上要錶現在加速蠕變階段,但各嚮異性程度比低溫高應力時顯著降低.存高溫低應力條件下,2種取嚮閤金中γ'相均已形筏,[001]取嚮閤金的筏化方嚮垂直于應力軸,而[011]取嚮閤金的筏化方嚮與應力軸的夾角約為45°.γ'相形筏後,阻礙瞭位錯運動,導緻加工硬化,因此,γ'相筏化是各嚮異性程度降低的主要原因.在[011]取嚮閤金的蠕變後期觀察到攣品組織同時穿越γ和γ'相,導緻試樣塑性人幅度降低,迅速斷裂.
분별제비료[001]화[011]취향적Ni-Co-Cr-Mo-w-Al-Ti-Ta얼기단정고온합금시양.재750℃/750 MPa조건하,[001]취향합금적평균연변수명규현고우[011]취향합금,[011]취향합금연신솔초고.재982℃/248 MPa조건하,[001]취향합금적평균연변수명화연신솔균고우[011]취향합금,각향이성상요표현재가속연변계단,단각향이성정도비저온고응력시현저강저.존고온저응력조건하,2충취향합금중γ'상균이형벌,[001]취향합금적벌화방향수직우응력축,이[011]취향합금적벌화방향여응력축적협각약위45°.γ'상형벌후,조애료위착운동,도치가공경화,인차,γ'상벌화시각향이성정도강저적주요원인.재[011]취향합금적연변후기관찰도련품조직동시천월γ화γ'상,도치시양소성인폭도강저,신속단렬.
Constant load creep tests were performed on the [001] and [011] oriented Ni-Co-Cr Mo W A1 Ti-Ta single crystal superalloys. The [001] oriented alloy has much longer creep lifc than that of [011] oriented alloy, but the elongation of [011] oriented alloy is slightly higher under the condition of 750 ℃/750 Mpa. The average creep life and elongation of [001] oriented alloy are both higher than that of [011] oriented alloy at 982 ℃/248 Mpa, and the anisotropy occurs mainly during the accelerating creep stage, but anisotropic degree decreases obviously. The SEM analysis reveals γ' phases are rafted in the two directions, which blocks the glide/climb of dislocations and causes creep hardening, the rafting of γ' phase is the dominant reason to decrease of crccp anisotropy at higher temperature. The TEM observation indicates deformation twins formed in [011] oriented alloy, whichlowers the plasticity of the sample and induces the sample to fracture rapidly.