贵阳医学院学报
貴暘醫學院學報
귀양의학원학보
JOURNAL OF GUIYANG MEDICAL COLLEGE
2001年
2期
134-135
,共2页
王海宁%杨永东%黄作苏
王海寧%楊永東%黃作囌
왕해저%양영동%황작소
靛蓝%色谱法,液相%感冒炎咳灵糖浆
靛藍%色譜法,液相%感冒炎咳靈糖漿
전람%색보법,액상%감모염해령당장
目的：建立感冒炎咳灵糖浆中靛蓝的含量测定。方法：采用高效液相色谱法测定感冒炎咳灵糖浆中靛蓝的含量。使用C18柱，甲醇∶水∶醋酸(68∶32∶0.5)为流动相，检测波长为280 nm。结果：线性关系良好，平均加样回收率为97.6%，相对偏差(RSD)=1.69%。结论：本方法精密度高，分离度良好，可用于感冒炎咳灵糖浆质量控制。
目的：建立感冒炎咳靈糖漿中靛藍的含量測定。方法：採用高效液相色譜法測定感冒炎咳靈糖漿中靛藍的含量。使用C18柱，甲醇∶水∶醋痠(68∶32∶0.5)為流動相，檢測波長為280 nm。結果：線性關繫良好，平均加樣迴收率為97.6%，相對偏差(RSD)=1.69%。結論：本方法精密度高，分離度良好，可用于感冒炎咳靈糖漿質量控製。
목적：건립감모염해령당장중전람적함량측정。방법：채용고효액상색보법측정감모염해령당장중전람적함량。사용C18주，갑순∶수∶작산(68∶32∶0.5)위류동상，검측파장위280 nm。결과：선성관계량호，평균가양회수솔위97.6%，상대편차(RSD)=1.69%。결론：본방법정밀도고，분리도량호，가용우감모염해령당장질량공제。
Objective:Assay of indigo in Gan Mao Yian Ke Ling Syrup. Methods: Determination of the contents of indigo in Gan Mao Yian Ke Ling Syrup with HPLC. This system consisted of C18 column and methanol-water-acetic acid (68∶32∶0.5) mixture as mobile phase, with the detection wavelength at 280 nm. Results: There is a good linear correlation.The avevage added recovery was 97.6%.RSD=1.69%. Conclusion: The method is accurate and capable of being used for the quality control of the syrup.
