辐射研究与辐射工艺学报
輻射研究與輻射工藝學報
복사연구여복사공예학보
JOURNAL OF RADIATION RESEARCH AND RADIATION PROCESSING
2005年
6期
325-328
,共4页
张雪平%周瑞敏%何林峰%饶卫红%陈永康%辛立辉
張雪平%週瑞敏%何林峰%饒衛紅%陳永康%辛立輝
장설평%주서민%하림봉%요위홍%진영강%신립휘
Fe3O4纳米粒子%电子束辐照%聚乙烯醇%聚乙二醇
Fe3O4納米粒子%電子束輻照%聚乙烯醇%聚乙二醇
Fe3O4납미입자%전자속복조%취을희순%취을이순
Fe3O4 nano-particles%EB irradiation%Polyvinyl alcohol (PVA)%Polyethylene glycol (PEG)
常温常压下不加入任何催化剂,用两种不同的活性剂聚乙烯醇(Polyvinyl alcohol,PVA)和聚乙二醇(Polyethylene glycol,PEG),在水溶液中通过电子束辐照可以成功地制备纳米Fe3O4粒子.通过紫外可见光分光光度计(Ultraviolet-visible spectrophotometer,UV)、X射线衍射(X-ray diffraction)、透射电子显微镜(Transmission electron microscopy,TEM)对辐照后的样品的光学特性、结构、形貌、大小进行表征.发现不同的活性剂对纳米粒子的尺寸会产生影响.
常溫常壓下不加入任何催化劑,用兩種不同的活性劑聚乙烯醇(Polyvinyl alcohol,PVA)和聚乙二醇(Polyethylene glycol,PEG),在水溶液中通過電子束輻照可以成功地製備納米Fe3O4粒子.通過紫外可見光分光光度計(Ultraviolet-visible spectrophotometer,UV)、X射線衍射(X-ray diffraction)、透射電子顯微鏡(Transmission electron microscopy,TEM)對輻照後的樣品的光學特性、結構、形貌、大小進行錶徵.髮現不同的活性劑對納米粒子的呎吋會產生影響.
상온상압하불가입임하최화제,용량충불동적활성제취을희순(Polyvinyl alcohol,PVA)화취을이순(Polyethylene glycol,PEG),재수용액중통과전자속복조가이성공지제비납미Fe3O4입자.통과자외가견광분광광도계(Ultraviolet-visible spectrophotometer,UV)、X사선연사(X-ray diffraction)、투사전자현미경(Transmission electron microscopy,TEM)대복조후적양품적광학특성、결구、형모、대소진행표정.발현불동적활성제대납미입자적척촌회산생영향.
Fe3O4 nano-particles have been successfully prepared by EB irradiation with two different actived agents, Polyvinyl alcohol (PVA) and Polyethylene glycol (PEG), at room temperature and ambient pressure, without any kind of catalysts. The optical properties, component and morphology of the irradiated samples were measured by Ultraviolet-visible spectrophotometer (UV-vis), X-ray diffraction (XRD) and Transmission electron microscopy (TEM). The size of nano particles was found to be affected by the action of the different actived agents.