一种新颖一维铅碘聚合物[(Pb2I5)(L-H+)·2DMF]n(L=Piperazine)的自组装合成和晶体结构
일충신영일유연전취합물[(Pb2I5)(L-H+)·2DMF]n(L=Piperazine)적자조장합성화정체결구
The Self-assembly Synthesis and Structure of a Novel 1-D Lead Iodide Adduct: [(Pb2I5)(L-H+)· 2DMF]n (L=Piperazine)
  • 万方数据
    无机化学学报 무궤화학학보
    JOURNAL OF INORGANIC CHEMISTRY
    2005年 1期 83-86 ,共4页

    李浩宏%陈之荣%黄长沧%赵斌%肖荣平%倪朝霞

    리호굉%진지영%황장창%조빈%초영평%예조하

    配位聚合物%有机-无机杂化%碘化铅%X-射线单晶衍射结构 配位聚閤物%有機-無機雜化%碘化鉛%X-射線單晶衍射結構
    배위취합물%유궤-무궤잡화%전화연%X-사선단정연사결구
    coordination polymers%lead iodide%organic-inorganic hybrid%X-ray single crystal structure


    The lead iodide adduct [(Pb2I5)(L-H+) ·2DMF]n (L=piperazine) has been prepared by self-assembly and structurally characterized. It presents one dimensional structure and crystallizes in Triclinic, P1 space group with the crystal cell parameter: a=0.92206(18) nm, b=1.237 5(3) nm, c=1.297 2(3) nm,α=99.05(3)°, β=102.98(3)°, y=mula C16H43NsO4Pb4I10 and Mr=2 509.39, the final R=0.053 3 and wR=O.146 4 for 3 889 observed reflections with I＞2σ(Ⅰ). CCDC: 250760.
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