CAJ | 학술논문

建立了食用菌中10种农药残留量的气相色谱分析方法.样品用乙酸乙酯-正己烷（体积比1∶1）溶液提取,经HP-5石英毛细管柱分离后,采用GC-FPD同时测定10种农药残留量.10种农药在0.1～5 mg/L范围内,均有良好线性关系.相关系数r大于0.997,样品在3个添加水平时的回收率为82%～110%,相对标准偏差为4.1%～12.9%.检出限为0.02～0.03 mg/kg.方法简便、快速、净化效果较好,可同时满足进、出口食用菌中多种农药残留量的检测需要.
건립료식용균중10충농약잔류량적기상색보분석방법.양품용을산을지-정기완（체적비1∶1）용액제취,경HP-5석영모세관주분리후,채용GC-FPD동시측정10충농약잔류량.10충농약재0.1～5 mg/L범위내,균유량호선성관계.상관계수r대우0.997,양품재3개첨가수평시적회수솔위82%～110%,상대표준편차위4.1%～12.9%.검출한위0.02～0.03 mg/kg.방법간편、쾌속、정화효과교호,가동시만족진、출구식용균중다충농약잔류량적검측수요.
A gas chromatography（GC） method is built for determination of ten pesticides residues in edible Fungi sample.The sample is extracted with ethyl acetaten-hexane（1∶1 by volume） then determined by gas chromatography using capillary column equipped with electron capture detector.The calibration curves show good linearity in the range of 0.1~5 mg/L for all ten pesticides,respectively,with correlative coefficients more than 0.997.The limits of detection（LOD） are 0.02~0.03 mg/kg for 10 pesticides in edible fungus.The recoveries of 10 pesticides from edible fungi sample with three concentration levels range from 82% to 110%,and the relative standard deviations are between 4.1% and 12.9%.The method is simple,fast,accurate and has better purification effect.It meets the requirements for simultaneous determination of many pesticides in edible fungi for import and export inspection.