光子学报
光子學報
광자학보
ACTA PHOTONICA SINICA
2012年
8期
922-926
,共5页
林建平%林丽梅%关贵清%吴扬微%赖发春
林建平%林麗梅%關貴清%吳颺微%賴髮春
림건평%림려매%관귀청%오양미%뢰발춘
磁控溅射%铬薄膜%结构%光学性质%电学性质
磁控濺射%鉻薄膜%結構%光學性質%電學性質
자공천사%락박막%결구%광학성질%전학성질
Magnetron sputtering%Cr film%Structure%Optical properties%Electrical properties
用直流磁控溅射技术在石英基片上制备不同厚度(5 nm~114 nm之间)的铬膜.使用X射线衍射仪和分光光度计分别检测薄膜的结构和光学性质,利用德鲁特模型和薄膜的透射、反射光谱计算铬膜的厚度和光学常量,并采用Van der Pauw方法测量薄膜电学性质.结果表明:制备的铬薄膜为体心立方的多晶态,随着膜厚的增加,薄膜的结晶性能提高,晶粒尺寸增大;在可见光区域,当膜厚小于32 nm时,随着膜厚的增加,折射率快速减小,消光系数快速增大,当膜厚大于32 nm时,折射率和消光系数均缓慢减小并逐渐趋于稳定;薄膜电阻率随膜厚的增加为一次指数衰减.
用直流磁控濺射技術在石英基片上製備不同厚度(5 nm~114 nm之間)的鉻膜.使用X射線衍射儀和分光光度計分彆檢測薄膜的結構和光學性質,利用德魯特模型和薄膜的透射、反射光譜計算鉻膜的厚度和光學常量,併採用Van der Pauw方法測量薄膜電學性質.結果錶明:製備的鉻薄膜為體心立方的多晶態,隨著膜厚的增加,薄膜的結晶性能提高,晶粒呎吋增大;在可見光區域,噹膜厚小于32 nm時,隨著膜厚的增加,摺射率快速減小,消光繫數快速增大,噹膜厚大于32 nm時,摺射率和消光繫數均緩慢減小併逐漸趨于穩定;薄膜電阻率隨膜厚的增加為一次指數衰減.
용직류자공천사기술재석영기편상제비불동후도(5 nm~114 nm지간)적락막.사용X사선연사의화분광광도계분별검측박막적결구화광학성질,이용덕로특모형화박막적투사、반사광보계산락막적후도화광학상량,병채용Van der Pauw방법측량박막전학성질.결과표명:제비적락박막위체심립방적다정태,수착막후적증가,박막적결정성능제고,정립척촌증대;재가견광구역,당막후소우32 nm시,수착막후적증가,절사솔쾌속감소,소광계수쾌속증대,당막후대우32 nm시,절사솔화소광계수균완만감소병축점추우은정;박막전조솔수막후적증가위일차지수쇠감.
Chromium (Cr) thin films with thickness ranging from 5 nm to 114 nm were deposited on quartz substrates by the direct current magnetron sputtering. X-ray diffraction and optical spectrophotometer were employed to characterize the crystal structure and optical properties,respectively.Based on the Drude optical dielectric model,optical constants and thicknesses of the films were calculated from the transmittance and reflectance data. The sheet resistance was measured by Van der Pauw method.The results show that the films have a body-centered cubic crystalline structure. The grain size of the film increases gradually and the crystalline performance enhances as film thickness increases. When film thickness is less than 32 nm,transmittance decreases sharply,reflectance and extinction coefficient increase rapidly as the increase of thickness.When thickness is larger than 32 nm,both refractive index and extinction coefficient decrease gradually until they become stable as the thickness increases.Resistivity is the first order exponential decay when thickness increases from 5 nm to 114 nm.