山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2011年
7期
27-29
,共3页
双格氏试剂%双齿膦配体%有机合成
雙格氏試劑%雙齒膦配體%有機閤成
쌍격씨시제%쌍치련배체%유궤합성
di - Grignard reagents%bidentate phosphine ligands%organic synthesis
介绍了一种简单实用的合成双二苯基膦烷烃的方法,并详细报道了合成路线,讨论了影响产率的各种因素。对最终产物进行了核磁表征,并对核磁谱图进行了解析。
介紹瞭一種簡單實用的閤成雙二苯基膦烷烴的方法,併詳細報道瞭閤成路線,討論瞭影響產率的各種因素。對最終產物進行瞭覈磁錶徵,併對覈磁譜圖進行瞭解析。
개소료일충간단실용적합성쌍이분기련완경적방법,병상세보도료합성로선,토론료영향산솔적각충인소。대최종산물진행료핵자표정,병대핵자보도진행료해석。
One simple and practical method for the synthesis of di (diphenylphosphine) - alkanes was introduced, and the synthesis route was reported in detail. Some influence factors were discussed here. Final products detected by 1↑H NMR, and 31↑P NMR were analysed.