宁德师范学院学报:自然科学版
寧德師範學院學報:自然科學版
저덕사범학원학보:자연과학판
Journal of Ningde Teachers College(Natural Science)
2011年
4期
357-360,375
,共5页
吴玉云%陈宝玲%潘青山%郑柳萍%颜桂炀
吳玉雲%陳寶玲%潘青山%鄭柳萍%顏桂煬
오옥운%진보령%반청산%정류평%안계양
共掺杂%TiO2%吸附剂%制备%表征
共摻雜%TiO2%吸附劑%製備%錶徵
공참잡%TiO2%흡부제%제비%표정
co-doped%TiO2%adsorbent%preparation%characterization
采用共沉淀法和水热法分别制备了铁、钒和银、碳的双组分共掺杂改性TiO2吸附剂Fe-V-TiO2和Ag-C-TiO2,并分别以亚甲基蓝和活性艳红X-3B为目标物来评价吸附剂的活性;采用XRD、FT-IR、SEM等现代手段对吸附剂的理化性能进行详细表征.结果表明,成功制备了Fe-V-TiO2和Ag-C-TiO2纳米高效吸附剂,其吸附具有一定的选择性;吸附处理30 min,前者对100 ppm亚甲基蓝的脱色率达95.86%,后者对50 ppm活性艳红X-3B的脱色率达92.06%.
採用共沉澱法和水熱法分彆製備瞭鐵、釩和銀、碳的雙組分共摻雜改性TiO2吸附劑Fe-V-TiO2和Ag-C-TiO2,併分彆以亞甲基藍和活性豔紅X-3B為目標物來評價吸附劑的活性;採用XRD、FT-IR、SEM等現代手段對吸附劑的理化性能進行詳細錶徵.結果錶明,成功製備瞭Fe-V-TiO2和Ag-C-TiO2納米高效吸附劑,其吸附具有一定的選擇性;吸附處理30 min,前者對100 ppm亞甲基藍的脫色率達95.86%,後者對50 ppm活性豔紅X-3B的脫色率達92.06%.
채용공침정법화수열법분별제비료철、범화은、탄적쌍조분공참잡개성TiO2흡부제Fe-V-TiO2화Ag-C-TiO2,병분별이아갑기람화활성염홍X-3B위목표물래평개흡부제적활성;채용XRD、FT-IR、SEM등현대수단대흡부제적이화성능진행상세표정.결과표명,성공제비료Fe-V-TiO2화Ag-C-TiO2납미고효흡부제,기흡부구유일정적선택성;흡부처리30 min,전자대100 ppm아갑기람적탈색솔체95.86%,후자대50 ppm활성염홍X-3B적탈색솔체92.06%.
Two double component co-doped adsorbents,Fe-V-TiO2 and Ag-C-TiO2,were obtained by coprecipitation and hydrothermal method.Methylene blue and reactive brilliant red X-3B were used as target to evaluate their property respectively.The physicochemical properties of the adsorbents were characterized by XRD,FTIR and SEM.The results showed that Fe-V-TiO2 and Ag-C-TiO2 nano-adsorbents with high efficiency were successful prepared,and they have a certain selectivity.After adsorbing 30 minutes,the decolour rate of Fe-V-TiO2 for methylene blue (100 ppm) was up to 95.86% and Ag-C-TiO2 for reactive brilliant red X-3B (50 ppm) was 92.06%.