化学工程与装备
化學工程與裝備
화학공정여장비
CHEMICAL ENGINEERING & EQUIPMENT
2010年
12期
143-146
,共4页
原油%酸值%测定%电位滴定
原油%痠值%測定%電位滴定
원유%산치%측정%전위적정
crude oil%acid value%determination%potentiometric titration
介绍了国内外测定石油及石油产品酸值的主要标准方法,比较了它们的特点、差别。以环烷基的高酸原油绥中36-1和石蜡基的高酸原油达尔原油为测定对象,用GB/T263(颜色法)与GB/T7304(电位滴定法)进行了对比试验,得出电位滴定法更加适合测定原油、渣油和其它石油产品的酸值。并在GB/T263(颜色法)的基础上进行了改进,改进后的方法用来测定环烷基高酸原油,测得的酸值结果与电位滴定基本一致,改进后的方法具有快速、简便、易操作的特点,有利于在实验室应用。
介紹瞭國內外測定石油及石油產品痠值的主要標準方法,比較瞭它們的特點、差彆。以環烷基的高痠原油綏中36-1和石蠟基的高痠原油達爾原油為測定對象,用GB/T263(顏色法)與GB/T7304(電位滴定法)進行瞭對比試驗,得齣電位滴定法更加適閤測定原油、渣油和其它石油產品的痠值。併在GB/T263(顏色法)的基礎上進行瞭改進,改進後的方法用來測定環烷基高痠原油,測得的痠值結果與電位滴定基本一緻,改進後的方法具有快速、簡便、易操作的特點,有利于在實驗室應用。
개소료국내외측정석유급석유산품산치적주요표준방법,비교료타문적특점、차별。이배완기적고산원유수중36-1화석사기적고산원유체이원유위측정대상,용GB/T263(안색법)여GB/T7304(전위적정법)진행료대비시험,득출전위적정법경가괄합측정원유、사유화기타석유산품적산치。병재GB/T263(안색법)적기출상진행료개진,개진후적방법용래측정배완기고산원유,측득적산치결과여전위적정기본일치,개진후적방법구유쾌속、간편、역조작적특점,유리우재실험실응용。
Important international and domestic standard test methods for acid number of petroleum and petroleum products were introduced, and compared their characteristics, the difference. With high acid naphthenic crude oil Suizhong 36-1 and high acid paraffin base Dahl crude oil is determined object, GB/T263 (indicator method) and GB/T7304 (potentiometric titration) were compared. It is concluded that GB/T7304 are suggested to determine the acid number of crude oil, residual oil and other petroleum products. It has been improved on the GB/T263 (indicator method) ,and the improved method is used to determine a high acid naphthenic crude oil, and the results are basically consistent with the potentiometric titration. The improved method has these features :fast, simple, easy to operate and so on.Therefore, it is conducive to applications in the laboratory.