日用化学工业
日用化學工業
일용화학공업
CHINA SURFACTANT DETERGENT & CONSMETICS
2010年
2期
148-152
,共5页
周相娟%赵玉琪%李伟%谢精精
週相娟%趙玉琪%李偉%謝精精
주상연%조옥기%리위%사정정
化妆品%气相色谱-质谱法%邻苯二甲酸酯
化妝品%氣相色譜-質譜法%鄰苯二甲痠酯
화장품%기상색보-질보법%린분이갑산지
cosmetic%gas chromatography-mass spectrometry (GC- MS)%phthalic ester
建立了气相色谱-质谱法同时测定化妆品中16种邻苯二甲酸酯的分析方法.在邻苯二甲酸酯质量浓度为0.1 mg/L~100 mg/L范围内,该方法测得的峰面积值与邻苯二甲酸酯的质量浓度的线性关系良好.线性相关系数均大于0.99,检出限为0.5 mg/kg,回收率为83.3%~121.8%,相对标准偏差为0.5%~6.4%.
建立瞭氣相色譜-質譜法同時測定化妝品中16種鄰苯二甲痠酯的分析方法.在鄰苯二甲痠酯質量濃度為0.1 mg/L~100 mg/L範圍內,該方法測得的峰麵積值與鄰苯二甲痠酯的質量濃度的線性關繫良好.線性相關繫數均大于0.99,檢齣限為0.5 mg/kg,迴收率為83.3%~121.8%,相對標準偏差為0.5%~6.4%.
건립료기상색보-질보법동시측정화장품중16충린분이갑산지적분석방법.재린분이갑산지질량농도위0.1 mg/L~100 mg/L범위내,해방법측득적봉면적치여린분이갑산지적질량농도적선성관계량호.선성상관계수균대우0.99,검출한위0.5 mg/kg,회수솔위83.3%~121.8%,상대표준편차위0.5%~6.4%.
A gas chromatography-mass spectrometry method was developed for the simultaneous determination of sixteen kinds of phthalic ester in cosmetics.Within range of phthalic ester concentration of 0.1 mg/L~100 mg/L, the peak area measured by this method has a good relationship with the phthalic ester concentration. All correlation coefficients are higher than 0.99.The detection limits achieves 0.5 mg/kg.The average recovery of sixteen kinds of phthalic ester is 83.3%~121.8% with the relative standard deviation of 0.5%~6.4%.