合成化学
閤成化學
합성화학
CHINESE JOURNAL OF SYNTHETIC CHEMISTRY
2010年
2期
219-221,225
,共4页
3,6-二溴环己烯%合成%构型%构象
3,6-二溴環己烯%閤成%構型%構象
3,6-이추배기희%합성%구형%구상
3,6-dibromocyclohexene%synthesis%configuration%conformation
报道一种新的立体选择性合成反式3,6-二溴环己烯的简易方法.环己烯与NBS在四氯化碳中回流反应30 min合成了反式3,6-二溴环己烯,其结构经~1H NMR, ~(13)C NMR, GC-MS及H-H COSY确证.
報道一種新的立體選擇性閤成反式3,6-二溴環己烯的簡易方法.環己烯與NBS在四氯化碳中迴流反應30 min閤成瞭反式3,6-二溴環己烯,其結構經~1H NMR, ~(13)C NMR, GC-MS及H-H COSY確證.
보도일충신적입체선택성합성반식3,6-이추배기희적간역방법.배기희여NBS재사록화탄중회류반응30 min합성료반식3,6-이추배기희,기결구경~1H NMR, ~(13)C NMR, GC-MS급H-H COSY학증.
Reported in this article is a new facile method for stereoselective synthesis of trans-3,6-dibromocyclohexene by bromination of cyclohexene with NBS at refluxing for 30 min in CCl_4. The structure was identified by ~1HNMR, 13C NMR, GC-MS and H-H COSY.
