CAJ | 학술논문

以丙醇锆为锆源,有机小分子三乙醇胺作为络合稳定剂和模板剂,通过水热合成途径制备了二氧化锆介孔分子筛.利用X射线粉末衍射和低温N2吸-脱附法等表征手段,考察了TEA加入量对二氧化锆介孔分子筛结构的影响,并探析了TEA在介观结构形成过程中的作用机理.
이병순고위고원,유궤소분자삼을순알작위락합은정제화모판제,통과수열합성도경제비료이양화고개공분자사.이용X사선분말연사화저온N2흡-탈부법등표정수단,고찰료TEA가입량대이양화고개공분자사결구적영향,병탐석료TEA재개관결구형성과정중적작용궤리.
With propanol zirconium as zirconium source and triethanolamine of organic small molecules as stabilizer and template of complexation,a mesoporous zirconium oxide has been made by hydrothermal synthesis.By means of X-ray and N2 adsorption-desorption analysis,the effect of TEA amount on the structure of mesoporous zirconium has been investigated,and related mechanism was also discussed.