中国有色金属学会会刊（英文版）
中國有色金屬學會會刊（英文版）
중국유색금속학회회간（영문판）
TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA
2006年
z1期
11-19
,共9页
superconductor%Bi-2223%magnetic fields%texture
The microstructure and superconducting properties of Bi-2223 superconductor fabricated in high magnetic fields were investigated. The results shows that the Bi-2212 grains with their c-axis parallel to the magnetic field were formed after the partial-melting and solidification in 8 T magnetic field,and transformed into the Bi-2223 grains with c-axis alignment during the further sintering process at 840 ℃ without magnetic field. The conversion of Bi-2212 grains to Bi-2223 grains has the heredity in grain alignment. The mixed structures of the Bi-2223 and the Bi-2212 grains with their c-axis parallel to the magnetic field are formed in samples sintered at 850-855 ℃ in 10 T magnetic field. When sintered in 10 T below 845 ℃,a high proportion of Bi-2223 phase is obtained,however no preferred orientation is observed. The Bi-2223 grains with their c-axis parallel to the axial direction of the vertical tube furnace are formed not only on the surface,but also in the center of the sample sintered at 850 ℃ for 120 h in a 15 ℃/cm temperature gradient without magnetic field. Moreover,the samples sintered in the temperature gradient and in a 10 T magnetic field have a stronger c-axis alignment of Bi-2223 phase.
