酿酒科技
釀酒科技
양주과기
LIQUOR-MAKING SCIENCE & TECHNOLOGY
2011年
10期
95-97
,共3页
任学坤%殷微微%徐文平%李小为%高凤文
任學坤%慇微微%徐文平%李小為%高鳳文
임학곤%은미미%서문평%리소위%고봉문
气相色谱%白酒%四甲基吡嗪%外标法
氣相色譜%白酒%四甲基吡嗪%外標法
기상색보%백주%사갑기필진%외표법
gas chromatography%liquor%tetramethylpyrazine%external standard method
建立了用气相色谱法测定白酒中四甲基吡嗪含量的方法,并对3种不同酒样进行检测。该外标法在测定酒样时的标准偏差为0.005~0.058,变异系数为2.83%~9.99%,回收率为86%~106%,具有操作简便快捷、精密度好、准确度高的特点。检测结果表明,不同酒样中的四甲基吡嗪的含量有较大差异,可以据此对白酒品质进行评价。
建立瞭用氣相色譜法測定白酒中四甲基吡嗪含量的方法,併對3種不同酒樣進行檢測。該外標法在測定酒樣時的標準偏差為0.005~0.058,變異繫數為2.83%~9.99%,迴收率為86%~106%,具有操作簡便快捷、精密度好、準確度高的特點。檢測結果錶明,不同酒樣中的四甲基吡嗪的含量有較大差異,可以據此對白酒品質進行評價。
건립료용기상색보법측정백주중사갑기필진함량적방법,병대3충불동주양진행검측。해외표법재측정주양시적표준편차위0.005~0.058,변이계수위2.83%~9.99%,회수솔위86%~106%,구유조작간편쾌첩、정밀도호、준학도고적특점。검측결과표명,불동주양중적사갑기필진적함량유교대차이,가이거차대백주품질진행평개。
We had developed the method of measuring tetramethylpyrazine content in liquor by GC.In this study,we had detected three different kinds of liquor samples.The standard deviation of external standard method was 0.005~0.058 in the measurement of liquor samples,the coefficient of variation was between 2.83 %~9.99 %,and the recovery was between 86 %~106 %.Such method had the advantages including simple and rapid operation,good precision,and high accuracy.The measurement results suggested that there was great different in tetramethylpyrazine content in different liquor samples,which could be used to evaluate liquor quality.