时珍国医国药
時珍國醫國藥
시진국의국약
LISHIZHEN MEDICINE AND MATERIA MEDICA RESEARCH
2001年
2期
132-133
,共2页
林宗玲%李倚岳%黄树亮%陈卡佳
林宗玲%李倚嶽%黃樹亮%陳卡佳
림종령%리의악%황수량%진잡가
胆石通胶囊%大黄提取工艺%大黄素%水温浸-乙醇回流法
膽石通膠囊%大黃提取工藝%大黃素%水溫浸-乙醇迴流法
담석통효낭%대황제취공예%대황소%수온침-을순회류법
通过大黄多种提取工艺的比较(水温浸法,乙醇回流法,水温浸-乙醇回流法),以大黄素为指标成分,采用薄层扫描法测定大黄素提取率,寻求生产胆石通胶囊大黄合适的提取工艺。结果表明,用水温浸-乙醇回流法提取大黄浸膏,能降低胆石通胶囊对大黄生药内控含量标准的要求,有利于大批量生产。
通過大黃多種提取工藝的比較(水溫浸法,乙醇迴流法,水溫浸-乙醇迴流法),以大黃素為指標成分,採用薄層掃描法測定大黃素提取率,尋求生產膽石通膠囊大黃閤適的提取工藝。結果錶明,用水溫浸-乙醇迴流法提取大黃浸膏,能降低膽石通膠囊對大黃生藥內控含量標準的要求,有利于大批量生產。
통과대황다충제취공예적비교(수온침법,을순회류법,수온침-을순회류법),이대황소위지표성분,채용박층소묘법측정대황소제취솔,심구생산담석통효낭대황합괄적제취공예。결과표명,용수온침-을순회류법제취대황침고,능강저담석통효낭대대황생약내공함량표준적요구,유리우대비량생산。
Several extraction methods for Rhubarb (water warm immersion,alcohol reflux,water-warm immersion-alcohol reflux) were compared in this study.The extraction yield of emodin as the content index were determined quantitatively by TLC-scanning to explore suitable extraction process for Rhubarb in Danshitong capsules. As a result, the water-warm immersion-alcohol reflux method is the optimum extraction process of Rhubarb in Danshitong capsules.