深圳大学学报(理工版)
深圳大學學報(理工版)
심수대학학보(리공판)
JOURNAL OF SHENZHEN UNIVERISYT SCIENCE & ENGINEERING
2010年
2期
211-216
,共6页
周晓明%辛红%游志军%陈艳媚%张培新
週曉明%辛紅%遊誌軍%陳豔媚%張培新
주효명%신홍%유지군%진염미%장배신
纳米材料%纳米结构薄膜%磷酸铈%纳米线%水浴陈化法%水热法
納米材料%納米結構薄膜%燐痠鈰%納米線%水浴陳化法%水熱法
납미재료%납미결구박막%린산시%납미선%수욕진화법%수열법
nanoporous material%nanostructure%CePO4%nanowire%bath aging%hydrothermal method
利用水浴陈化和水热法在栽玻片基底上合成了由CePO4纳米线构筑的纳米结构薄膜.研究两种水浴环境中不同合成时间对CePO4纳米结构形貌的影响.采用扫描电子显微镜(SEM)、X射线衍射仪(XRD)和热重-差示扫描热法(TG-DSC)对CePO4纳米结构进行表征,结果表明,在不同水浴环境中,CePO4纳米结构呈现不同形貌,且晶型结构、纳米线的长度和直径均有所改变.合成时间差异是CePO4纳米结构呈现不同形貌的重要因素之一.
利用水浴陳化和水熱法在栽玻片基底上閤成瞭由CePO4納米線構築的納米結構薄膜.研究兩種水浴環境中不同閤成時間對CePO4納米結構形貌的影響.採用掃描電子顯微鏡(SEM)、X射線衍射儀(XRD)和熱重-差示掃描熱法(TG-DSC)對CePO4納米結構進行錶徵,結果錶明,在不同水浴環境中,CePO4納米結構呈現不同形貌,且晶型結構、納米線的長度和直徑均有所改變.閤成時間差異是CePO4納米結構呈現不同形貌的重要因素之一.
이용수욕진화화수열법재재파편기저상합성료유CePO4납미선구축적납미결구박막.연구량충수욕배경중불동합성시간대CePO4납미결구형모적영향.채용소묘전자현미경(SEM)、X사선연사의(XRD)화열중-차시소묘열법(TG-DSC)대CePO4납미결구진행표정,결과표명,재불동수욕배경중,CePO4납미결구정현불동형모,차정형결구、납미선적장도화직경균유소개변.합성시간차이시CePO4납미결구정현불동형모적중요인소지일.
The nanostructured CePO4 films were prepared through the water bath aging and hydrothermal process in glass slide substrate.The effects of different water environment,different reaction time on the morphology of CePO4 nanostructures were discussed.The CePO4 nanostructures were characterized by scanning electron microscope(SEM), X-ray diffratometer(XRD), and thermogravimetry-differential scanning calorimetry(TG-DSC).These results indicate that the nanostructured CePO4 films present different patterns in different aquatic environments.The crystal structure,the length and diameter of CePO4 nanowires have been changed.Reaction time is an important factor influencing the patterns of nanostructured CePO4 films.