中国医院药学杂志
中國醫院藥學雜誌
중국의원약학잡지
CHINESE JOURNAL OF HOSPITAL PHARMACY
2001年
2期
75-77
,共3页
黄衍民%潘留华%洪伟%菅鹏%高曰胜%王晓先
黃衍民%潘留華%洪偉%菅鵬%高曰勝%王曉先
황연민%반류화%홍위%관붕%고왈성%왕효선
抗感冒片%绿原酸%薄层扫描法%含量测定
抗感冒片%綠原痠%薄層掃描法%含量測定
항감모편%록원산%박층소묘법%함량측정
目的:测定抗感冒片中绿原酸的含量。方法:用乙醇提取并制成供试品,以薄层扫描法测定,λs=333 nm,λR=220 nm。结果:平均回收率为98.7%,RSD=1.87%,三批样品中绿原酸的含量分别为2.455 mg/片,2.368 mg/片,2.262 mg/片。结论:本法简便、准确、灵敏,可作为该制剂的质量控制方法。
目的:測定抗感冒片中綠原痠的含量。方法:用乙醇提取併製成供試品,以薄層掃描法測定,λs=333 nm,λR=220 nm。結果:平均迴收率為98.7%,RSD=1.87%,三批樣品中綠原痠的含量分彆為2.455 mg/片,2.368 mg/片,2.262 mg/片。結論:本法簡便、準確、靈敏,可作為該製劑的質量控製方法。
목적:측정항감모편중록원산적함량。방법:용을순제취병제성공시품,이박층소묘법측정,λs=333 nm,λR=220 nm。결과:평균회수솔위98.7%,RSD=1.87%,삼비양품중록원산적함량분별위2.455 mg/편,2.368 mg/편,2.262 mg/편。결론:본법간편、준학、령민,가작위해제제적질량공제방법。
OBJECTIVE:To determine chlorogenic acid in Kangganmao tablets. METHODS:The tablets were extracted with alcohol, to prepare sample solution,then determinated by TLC scanning.RESULTS:Average recovery was 98.7%, RSD=1.87%,the contents of the chlorogenic cacid per tablet in three batches of samples were 2.455 mg, 2.368 mg and 2.262 mg respectively.CONCLUSIONS:The method can be used for the quality control of Kangganmao tablets.