中山大学学报(自然科学版)
中山大學學報(自然科學版)
중산대학학보(자연과학판)
ACTA SCIENTIARUM NATURALIUM UNIVERSITATIS SUNYATSENI
2009年
z2期
113-115
,共3页
王红斌%施金榆%宁平%杨敏%冯桂权
王紅斌%施金榆%寧平%楊敏%馮桂權
왕홍빈%시금유%저평%양민%풍계권
膨润土%负载型固体酸%表征
膨潤土%負載型固體痠%錶徵
팽윤토%부재형고체산%표정
bentonite%loaded solid acid%characterization
用无水浸渍法制备了膨润土负载型固体酸催化剂.通过XRD、BET、SEM、XPS等手段对催化剂进行表征分析.结果表明,负载物与膨润土有良好的结合性能,形成了新的物相或无定形状态.固体酸表面粗糙,有许多的微孔,表面的这种变化有利于在催化反应时,反应物向酸性中心靠近,提高催化活性,同时也使固体酸的稳定性提高.
用無水浸漬法製備瞭膨潤土負載型固體痠催化劑.通過XRD、BET、SEM、XPS等手段對催化劑進行錶徵分析.結果錶明,負載物與膨潤土有良好的結閤性能,形成瞭新的物相或無定形狀態.固體痠錶麵粗糙,有許多的微孔,錶麵的這種變化有利于在催化反應時,反應物嚮痠性中心靠近,提高催化活性,同時也使固體痠的穩定性提高.
용무수침지법제비료팽윤토부재형고체산최화제.통과XRD、BET、SEM、XPS등수단대최화제진행표정분석.결과표명,부재물여팽윤토유량호적결합성능,형성료신적물상혹무정형상태.고체산표면조조,유허다적미공,표면적저충변화유리우재최화반응시,반응물향산성중심고근,제고최화활성,동시야사고체산적은정성제고.
The paper deals with the preparatin of solid acid catalyst loaded on Bentonite through an impregnating method. The charac-teriozations of the catalysts were also analyzed with XRD, BET, SEM, XPS. The results show that the adhesiveness between Lewis acid and Bentonite is very good, and they have been formed new conditions. The whole structure becomes more loose and rugged. This change is helpful in the catalytic reaction, and can improve the catalytic activity and the stability of solid acid.