CAJ | 학술논문

采用可溶性Ni阳极电刷镀方法制备纳米晶Ni-Fe合金镀层,利用XRD、SEM、TEM、显微硬度计等测试方法分析低温退火对镀层结构和性能的影响.结果表明:纳米晶Ni-Fe合金镀层的硬度随退火温度的升高而提高,在200 ℃时达到最大值,存在明显的退火再强化;继续提高退火温度导致镀层硬度降低;400 ℃退火后的镀层硬度与镀态的接近;纳米晶Ni-Fe合金镀层退火过程没有出现晶粒异常长大,表现出比纯Ni镀层更高的热稳定性.
채용가용성Ni양겁전쇄도방법제비납미정Ni-Fe합금도층,이용XRD、SEM、TEM、현미경도계등측시방법분석저온퇴화대도층결구화성능적영향.결과표명:납미정Ni-Fe합금도층적경도수퇴화온도적승고이제고,재200 ℃시체도최대치,존재명현적퇴화재강화;계속제고퇴화온도도치도층경도강저;400 ℃퇴화후적도층경도여도태적접근;납미정Ni-Fe합금도층퇴화과정몰유출현정립이상장대,표현출비순Ni도층경고적열은정성.
Nanocrystalline Ni-Fe alloy coatings were synthesized by brush plating using soluble anode. Microhardness test and techniques of XRD, SEM and TEM were applied to characterize the microstructures and mechanical properties of Ni-Fe alloy coatings. The results show that the microhardness of Ni-Fe alloy coatings increases with increasing annealing temperature and reaches a peak value at 200 ℃, showing a significant hardening during annealing. With further increasing annealing temperature, the microhardness decreases gradually, but the microhardness of the coating after being annealed at 400 ℃ is still as high as that of the as-deposited sample. The abnormal grain growth is not observed during annealing of Ni-Fe alloy coatings, which indicates a better thermal stability.