天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2012年
4期
465-468
,共4页
李昌松%余红伟%陈晓珍%吴晓青%方冬梅%李国友
李昌鬆%餘紅偉%陳曉珍%吳曉青%方鼕梅%李國友
리창송%여홍위%진효진%오효청%방동매%리국우
四川溲疏%甾体%三萜%香豆素
四川溲疏%甾體%三萜%香豆素
사천수소%치체%삼첩%향두소
Deutxia setchuenensis%steroids%triterpenoids%coumarin
运用多种色谱技术从四川溲疏(Deutzia setchuenensis Franch)全草的95%乙醇提取物中首次分离到9个化合物.通过波谱方法和与已知品对照的手段将它们鉴定为:β-谷甾醇(1)、白桦酯酵(2)、hydrangetin(3)、齐墩果酸(4)、肉桂酸(5)、齐墩果酸-3-O-β-D-吡喃葡萄糖醛酸苷(6)、β-胡萝卜苷(7)、齐墩果酸-3-O-(β-D-吡喃葡萄糖醛酸-6-正丁酯)(8)和齐墩果酸-3-O-β-D-吡喃葡萄糖醛酸-28-P-β-D-吡喃葡萄糖苷(9).
運用多種色譜技術從四川溲疏(Deutzia setchuenensis Franch)全草的95%乙醇提取物中首次分離到9箇化閤物.通過波譜方法和與已知品對照的手段將它們鑒定為:β-穀甾醇(1)、白樺酯酵(2)、hydrangetin(3)、齊墩果痠(4)、肉桂痠(5)、齊墩果痠-3-O-β-D-吡喃葡萄糖醛痠苷(6)、β-鬍蘿蔔苷(7)、齊墩果痠-3-O-(β-D-吡喃葡萄糖醛痠-6-正丁酯)(8)和齊墩果痠-3-O-β-D-吡喃葡萄糖醛痠-28-P-β-D-吡喃葡萄糖苷(9).
운용다충색보기술종사천수소(Deutzia setchuenensis Franch)전초적95%을순제취물중수차분리도9개화합물.통과파보방법화여이지품대조적수단장타문감정위:β-곡치순(1)、백화지효(2)、hydrangetin(3)、제돈과산(4)、육계산(5)、제돈과산-3-O-β-D-필남포도당철산감(6)、β-호라복감(7)、제돈과산-3-O-(β-D-필남포도당철산-6-정정지)(8)화제돈과산-3-O-β-D-필남포도당철산-28-P-β-D-필남포도당감(9).
Nine compounds were isolated from the 95% ethanol extract of the whole plants of Deutzia setchuenensis Franch for the first time.On the basis of spectral data or by comparing with authentic samples,they were identified as β-sitosterol (1),betulin (2),hydrangetin (3),oleanolic acid (4),cinnamic acid (5),oleanolic acid 3-O-β-D-glucuro-nopyranoside (6),β-daucosterol (7),oleanolic acid 3-O-(β-D-glucuronopyranoside-6-O-butyl ester) (8) and oleanolic acid 3-O-β-D-glucuronopyranosyl-28-3-O-β-D-glucopyranoside (9).They were isolated from the plant for the first time.