CAJ | 학술논문

采用XRD、DSC、TEM等检测方法,研究了深冷循环处理、473K退火循环处理及冷-热循环处理对Fe_(68)Ni_1Al_5Ga_2P9 (6.5)B_(46)Si_3C_(6.75)非晶合金的微观结构、晶化过程及磁性能的影响.结果表明:经不同的循环处理后,试样仍然保持非晶结构,发生了结构弛豫,微观结构改变.但与淬态试样相比,玻璃转变温度、晶化温度及晶化峰值温度存在一定的变化.退火品化后,各试样中析出相的种类、数量、晶粒尺寸等有明显的不同.磁性能数据表明:品化后,循环处理的试样其磁性能较淬态有所提高.
채용XRD、DSC、TEM등검측방법,연구료심랭순배처리、473K퇴화순배처리급랭-열순배처리대Fe_(68)Ni_1Al_5Ga_2P9 (6.5)B_(46)Si_3C_(6.75)비정합금적미관결구、정화과정급자성능적영향.결과표명:경불동적순배처리후,시양잉연보지비정결구,발생료결구이예,미관결구개변.단여쉬태시양상비,파리전변온도、정화온도급정화봉치온도존재일정적변화.퇴화품화후,각시양중석출상적충류、수량、정립척촌등유명현적불동.자성능수거표명:품화후,순배처리적시양기자성능교쉬태유소제고.
The effects of deep cryogenic cycle treatment, annealing at 473 K cycle treatment and cold-hot cycle treatment on the microstructure, magnetic properties and crystallization process of Fe_(68)Ni_1Al_5Ga_2P9 (6.5)B_(46)Si_3C_(6.75) amorphous alloys were studied by XRD, DSC and TEM. The results show that samples are still amorphous after different cycle treatment. Struture relaxstion occurs and the microstructure changes. But compared to as-quenched samples, the glass transition temperature, crystallization temperature and crystallization peak temperature have same changes. After annealing crystallization, there are some obvious differences in the variety, the amount and size of crystallization. The statistics of magnetic properties show that it has a little elevation compared to as-quenched samples.