天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2011年
6期
1017-1020
,共4页
赵万顺%高文远%黄贤校%黄璐琦%肖培根
趙萬順%高文遠%黃賢校%黃璐琦%肖培根
조만순%고문원%황현교%황로기%초배근
球药隔重楼%化学成分%甾体皂苷
毬藥隔重樓%化學成分%甾體皂苷
구약격중루%화학성분%치체조감
Paris fargesii Franch.%chemical constituents%steroidal saponins
采用硅胶柱层析、大孔吸附树脂、ODS柱层析、Sephadex LH-20和RP-C18柱层析等技术中分离得到8个化合物.通过波谱学数据和已知化合物数据比较,分别鉴定为β-谷甾醇(1),β-蜕皮激素(2),Paris Saponins Ⅴ(3),Paris Saponins Ⅰ (4),Paris SaponinsⅡ(5),Paris SaponinsⅦ(6),Paris Saponins H(7)和Paris SaponinsⅥ(8).化合物1~8均为首次从球药隔重楼中分离得到.
採用硅膠柱層析、大孔吸附樹脂、ODS柱層析、Sephadex LH-20和RP-C18柱層析等技術中分離得到8箇化閤物.通過波譜學數據和已知化閤物數據比較,分彆鑒定為β-穀甾醇(1),β-蛻皮激素(2),Paris Saponins Ⅴ(3),Paris Saponins Ⅰ (4),Paris SaponinsⅡ(5),Paris SaponinsⅦ(6),Paris Saponins H(7)和Paris SaponinsⅥ(8).化閤物1~8均為首次從毬藥隔重樓中分離得到.
채용규효주층석、대공흡부수지、ODS주층석、Sephadex LH-20화RP-C18주층석등기술중분리득도8개화합물.통과파보학수거화이지화합물수거비교,분별감정위β-곡치순(1),β-세피격소(2),Paris Saponins Ⅴ(3),Paris Saponins Ⅰ (4),Paris SaponinsⅡ(5),Paris SaponinsⅦ(6),Paris Saponins H(7)화Paris SaponinsⅥ(8).화합물1~8균위수차종구약격중루중분리득도.
Eight compounds were isolated and purified by solvent extraction,repeated chromatography with silica gel,Sephadex LH-20 and RP-C18 from Parisfargesii Franch.Then their structures were identified by spectral of analysis asβ-sitosterol(1),β-ecdysterone(2),Paris Saponins Ⅴ (3),Paris Saponins Ⅰ (4),Paris Saponins Ⅱ (5),Paris SaponinsⅦ (6),Paris Saponins H (7),Paris Saponins Ⅵ (8).Compounds 1-8 were isolated from Paris fargesii Franch for the first time.