微波辐射固相合成cis-和trans-3-(3,4-二羟基苄基)-六氢吡咯并[1,2-α]哌嗪-1,4-二酮
미파복사고상합성cis-화trans-3-(3,4-이간기변기)-륙경필각병[1,2-α]고진-1,4-이동
Synthesis of cis-and trans-3-(3,4-dihydroxybenzyl)-hexahydropyrrolo[1,2-α]piperazine-1,4-dione under Microwave Irradiation by Solid-phase
  • 万方数据
    合成化学 합성화학
    CHINESE JOURNAL OF SYNTHETIC CHEMISTRY
    2008年 4期 398-401,409 ,共5页

    张崇敬%张志辉%徐柏玲

    장숭경%장지휘%서백령

    微波辐射%二酮哌嗪%固相合成%硅胶吸附 微波輻射%二酮哌嗪%固相閤成%硅膠吸附
    미파복사%이동고진%고상합성%규효흡부
    将Boe-L-Pro-L-DOPA-OMe吸附在硅胶上,利用微波技术固相合成了cis-和trans-3-(3,4-二羟基苄基)-六氢吡咯并[1,2-α]哌嗪-1,4-二酮,合计收率70.2%,其结构经1H NMR,13C NMR和HR-MS表征.
    장Boe-L-Pro-L-DOPA-OMe흡부재규효상,이용미파기술고상합성료cis-화trans-3-(3,4-이간기변기)-륙경필각병[1,2-α]고진-1,4-이동,합계수솔70.2%,기결구경1H NMR,13C NMR화HR-MS표정.
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