中国有色金属学报
中國有色金屬學報
중국유색금속학보
THE CHINESE JOURNAL OF NONFERROUS METALS
2010年
1期
143-148
,共6页
李大武%孙挺%姚广春%张小明%李杰
李大武%孫挺%姚廣春%張小明%李傑
리대무%손정%요엄춘%장소명%리걸
泡沫铝%熔体发泡法%氢化锆%润湿性
泡沫鋁%鎔體髮泡法%氫化鋯%潤濕性
포말려%용체발포법%경화고%윤습성
foam aluminum%melt-based route%zirconium hydride%wettability
以ZrH_2为发泡剂,采用熔体发泡法制备铝基小孔径泡沫铝,分析其制备过程及影响孔结构的因素;优化实验室制备泡沫铝的工艺条件;借助图形分析方法表征泡沫铝的孔径分布,并与TiH_2制备的泡沫铝进行了对比;采用改进座滴装置研究铝合金与氢化物的润湿行为.结果表明:ZrH_2较适合制备小孔径泡沫铝;优化工艺条件为:Al 650 g,增粘剂Ca 的加入量2.5%,发泡剂ZrH_2的加入量1.0%,发泡温度680 ℃,搅拌时间1.5 min,保温时间2.5 min;制备的泡沫铝孔径均匀,平均孔径小于1.5 mm;ZrH_2在铝合金中的润湿特点是导致泡沫铝孔径较小的主要原因.
以ZrH_2為髮泡劑,採用鎔體髮泡法製備鋁基小孔徑泡沫鋁,分析其製備過程及影響孔結構的因素;優化實驗室製備泡沫鋁的工藝條件;藉助圖形分析方法錶徵泡沫鋁的孔徑分佈,併與TiH_2製備的泡沫鋁進行瞭對比;採用改進座滴裝置研究鋁閤金與氫化物的潤濕行為.結果錶明:ZrH_2較適閤製備小孔徑泡沫鋁;優化工藝條件為:Al 650 g,增粘劑Ca 的加入量2.5%,髮泡劑ZrH_2的加入量1.0%,髮泡溫度680 ℃,攪拌時間1.5 min,保溫時間2.5 min;製備的泡沫鋁孔徑均勻,平均孔徑小于1.5 mm;ZrH_2在鋁閤金中的潤濕特點是導緻泡沫鋁孔徑較小的主要原因.
이ZrH_2위발포제,채용용체발포법제비려기소공경포말려,분석기제비과정급영향공결구적인소;우화실험실제비포말려적공예조건;차조도형분석방법표정포말려적공경분포,병여TiH_2제비적포말려진행료대비;채용개진좌적장치연구려합금여경화물적윤습행위.결과표명:ZrH_2교괄합제비소공경포말려;우화공예조건위:Al 650 g,증점제Ca 적가입량2.5%,발포제ZrH_2적가입량1.0%,발포온도680 ℃,교반시간1.5 min,보온시간2.5 min;제비적포말려공경균균,평균공경소우1.5 mm;ZrH_2재려합금중적윤습특점시도치포말려공경교소적주요원인.
Foam aluminum with small pore diameters was prepared by the melt-based route using ZrH_2 as foaming agent. The relationship between the foaming process parameters and the cell structures of foam aluminum was studied. The foaming process conditions were optimized. The pore diameter distribution of the foam aluminum was characterized by the graphical analysis method and the foaming agent TiH_2 was commonly used for the comparison. The improved sessile drop device was used to research the wetting behaviors of Al alloy on the surface of hydride. The results indicate that the foaming agent ZrH_2 is suitable for preparation of the small pore diameter foam aluminum and the optimized process conditions are obtained (650 g of Al; addition of Ca 2.5%; ZrH_2 1.0%; temperature 680 ℃; stirring time 1.5 min; holding time 2.5 min). The average pore diameter is uniform and below 1.5 mm. The wetting behaviors are the main factor of influencing the pore diameter.