天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2011年
3期
404-409
,共6页
石菖蒲%天南星科%酚性成分%三萜
石菖蒲%天南星科%酚性成分%三萜
석창포%천남성과%분성성분%삼첩
运用色谱法从石菖蒲根茎提取物中分离得到18个化合物,经波谱学分析鉴定为:(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propylneolignan(1),(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propyheoligan-9-O-β-D-glucopyranoside(2),7'-bdroxylariciresinol-9-acetate(3),5-羟基-3,7,4'-三甲氧基黄酮(4),野漆树苷(5),紫云英苷(6),松属素-3-O-芸香糖苷(7),山奈酚-3-O-芸香糖苷(8),德钦红景天苷(9),isoschaftoside(10),5-羟甲基糠醛(11),反式桂皮酸(12),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oicacid(13),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester(14),环阿屯醇(15),胡萝卜苷(16),羽扇豆醇(17),(22E,24R)-ergosta-5,7,22-trien-3β-ol(18).除化合物4、11和16外,其余15个化合物均为首次从该植物中分离得到.
運用色譜法從石菖蒲根莖提取物中分離得到18箇化閤物,經波譜學分析鑒定為:(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propylneolignan(1),(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propyheoligan-9-O-β-D-glucopyranoside(2),7'-bdroxylariciresinol-9-acetate(3),5-羥基-3,7,4'-三甲氧基黃酮(4),野漆樹苷(5),紫雲英苷(6),鬆屬素-3-O-蕓香糖苷(7),山奈酚-3-O-蕓香糖苷(8),德欽紅景天苷(9),isoschaftoside(10),5-羥甲基糠醛(11),反式桂皮痠(12),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oicacid(13),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester(14),環阿屯醇(15),鬍蘿蔔苷(16),羽扇豆醇(17),(22E,24R)-ergosta-5,7,22-trien-3β-ol(18).除化閤物4、11和16外,其餘15箇化閤物均為首次從該植物中分離得到.
운용색보법종석창포근경제취물중분리득도18개화합물,경파보학분석감정위:(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propylneolignan(1),(7S,8R)-4,9'-dihydroxyl-3,3'-dimethoxyl-7,8-dihydrobenzofuran-1'-propyheoligan-9-O-β-D-glucopyranoside(2),7'-bdroxylariciresinol-9-acetate(3),5-간기-3,7,4'-삼갑양기황동(4),야칠수감(5),자운영감(6),송속소-3-O-예향당감(7),산내분-3-O-예향당감(8),덕흠홍경천감(9),isoschaftoside(10),5-간갑기강철(11),반식계피산(12),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oicacid(13),3,7-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester(14),배아둔순(15),호라복감(16),우선두순(17),(22E,24R)-ergosta-5,7,22-trien-3β-ol(18).제화합물4、11화16외,기여15개화합물균위수차종해식물중분리득도.
