榆林学院学报
榆林學院學報
유림학원학보
JOURNAL OF YULIN COLLEGE
2011年
4期
70-72
,共3页
卢翠英%张智芳%马亚军%王爱民
盧翠英%張智芳%馬亞軍%王愛民
로취영%장지방%마아군%왕애민
正交试验%离子液体%碳酸二甲酯%最佳合成工艺
正交試驗%離子液體%碳痠二甲酯%最佳閤成工藝
정교시험%리자액체%탄산이갑지%최가합성공예
orthogonal expenriment design%ionic liquids%dimethyl carbonate%idea synthesis conditions
以离子液体为介质,采用正交试验法确定尿素醇解法最佳合成碳酸二甲酯的条件,通过极差分析和方差分析法结果对比,最终确定尿素醇解法最佳合成碳酸二甲酯的条件是:150℃下,离子液体与尿素化学计算量比为2.0下合成7个小时。
以離子液體為介質,採用正交試驗法確定尿素醇解法最佳閤成碳痠二甲酯的條件,通過極差分析和方差分析法結果對比,最終確定尿素醇解法最佳閤成碳痠二甲酯的條件是:150℃下,離子液體與尿素化學計算量比為2.0下閤成7箇小時。
이리자액체위개질,채용정교시험법학정뇨소순해법최가합성탄산이갑지적조건,통과겁차분석화방차분석법결과대비,최종학정뇨소순해법최가합성탄산이갑지적조건시:150℃하,리자액체여뇨소화학계산량비위2.0하합성7개소시。
Dimethyl Carbonate were synthemed from urea and methanol in ionic liquids in the work..The highly productive conditions were explored by using orthogonal expenriment design.Through compareing the results of range analysis and variance analysis,the idea sythemitic conditions of dimethyl carbonate from urea and methanol in ionic liquid were as follows:at 150℃,at 1 of the ratio of ironic liquid to urea,and for 7 hours.